C₄₅H₅₂N₆O₆

Base Information

Chemical Name:C₄₅H₅₂N₆O₆
CAS No.:1262036-21-4
Molecular Formula:C₄₅H₅₂N₆O₆
Molecular Weight:772.944
Hs Code.:

C<sub>45</sub>H<sub>52</sub>N<sub>6</sub>O<sub>6</sub>

Synonyms:C₄₅H₅₂N₆O₆

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Chemical Property of C₄₅H₅₂N₆O₆

Chemical Property:

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Technology Process of C₄₅H₅₂N₆O₆

There total 27 articles about C₄₅H₅₂N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1242104-25-1
(2S,3aS,6R,7aS)-2-(4-azidobutylcarbamoyl)-1-((S)-2-((S)-2-(benzyloxy)-3-(4-(benzyloxy)phenyl)propanamido)-3-phenylpropanoyl)octahydro-1H-indol-6-yl acetate

: 1262036-21-4
C₄₅H₅₂N₆O₆

Guidance literature:: With methanol; lithium hydroxide monohydrate; water; In tetrahydrofuran; at 0 ℃; for 4h;
DOI:10.1021/ol1017189

Reference yield:

: 481072-37-1
(S)-3-(p-benzyloxyphenyl)lactic acid methyl ester

: 1262036-21-4
C₄₅H₅₂N₆O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: 1.5 h / 20 °C / Inert atmosphere

2.1: methanol; lithium hydroxide monohydrate / tetrahydrofuran; water / 3 h / 20 °C

3.1: triethylamine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C / Inert atmosphere

4.1: methanol; lithium hydroxide monohydrate / tetrahydrofuran; water / 0.5 h / 20 °C

5.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

6.1: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

7.1: cyclohexa-1,4-diene; N-methylcarbazole / tetrahydrofuran; water / 18 h / Inert atmosphere; UV-irradiation

8.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / acetonitrile / 2 h / Inert atmosphere

9.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

10.1: sodium azide / N,N-dimethyl-formamide / 50 °C

11.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 4 h / 0 °C

With methanol; dmap; sodium azide; N-methylcarbazole; lithium hydroxide monohydrate; cyclohexa-1,4-diene; tris(dimethylamino)sulfonium trimethylsilyldifluoride; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201400046

Reference yield:

: 162919-37-1
(S)-3-[4-(benzyloxy)phenyl]-2-hydroxypropanoic acid

: 1262036-21-4
C₄₅H₅₂N₆O₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: dichloromethane; methanol; diethyl ether / 0.25 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

2.2: 1.5 h / 20 °C / Inert atmosphere

3.1: methanol; lithium hydroxide monohydrate / tetrahydrofuran; water / 3 h / 20 °C

4.1: triethylamine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C / Inert atmosphere

5.1: methanol; lithium hydroxide monohydrate / tetrahydrofuran; water / 0.5 h / 20 °C

6.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

7.1: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

8.1: cyclohexa-1,4-diene; N-methylcarbazole / tetrahydrofuran; water / 18 h / Inert atmosphere; UV-irradiation

9.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / acetonitrile / 2 h / Inert atmosphere

10.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

11.1: sodium azide / N,N-dimethyl-formamide / 50 °C

12.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 4 h / 0 °C

With methanol; dmap; sodium azide; N-methylcarbazole; lithium hydroxide monohydrate; cyclohexa-1,4-diene; tris(dimethylamino)sulfonium trimethylsilyldifluoride; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201400046