(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-2,4,6-trimethylphenylsulfonamide

Base Information

Chemical Name:(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-2,4,6-trimethylphenylsulfonamide
CAS No.:1239456-72-4
Molecular Formula:C₂₅H₂₇NO₂S
Molecular Weight:405.561
Hs Code.:

Synonyms:(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-2,4,6-trimethylphenylsulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-2,4,6-trimethylphenylsulfonamide

Chemical Property:

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Technology Process of (E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-2,4,6-trimethylphenylsulfonamide

There total 4 articles about (E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-2,4,6-trimethylphenylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 673-32-5
1-Phenylprop-1-yne

: 200123-82-6
C₁₇H₁₈O₂S

: 1239456-72-4
(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-2,4,6-trimethylphenylsulfonamide

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; tributylphosphine; diethylzinc; In 1,2-dimethoxyethane; toluene; at 25 ℃; for 2h; chemoselective reaction;
DOI:10.1021/ja104505t

Reference yield:

: 673-32-5
1-Phenylprop-1-yne

: 85045-43-8
N-benzyl-2,4,6-trimethylbenzenesulfonamide

: 1239456-72-4
(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-2,4,6-trimethylphenylsulfonamide

: C₂₅H₂₇NO₂S

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium phosphate; dicyclohexylphenylphosphine; In 1,4-dioxane; at 120 ℃; for 24h; Overall yield = 95 percent; Overall yield = 38.7 mg; regioselective reaction; Inert atmosphere; Glovebox;
DOI:10.1021/jacs.1c00622

Reference yield:

: 100-46-9
benzylamine

: 1239456-72-4
(E)-N-(2-methyl-1,3-diphenylprop-2-enyl)-2,4,6-trimethylphenylsulfonamide

: C₂₅H₂₇NO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1.17 h / 0 - 20 °C / Inert atmosphere; Glovebox

2: bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium phosphate; dicyclohexylphenylphosphine / 1,4-dioxane / 24 h / 120 °C / Inert atmosphere; Glovebox

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium phosphate; triethylamine; dicyclohexylphenylphosphine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jacs.1c00622