octyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-D-arabinofuranoside

Base Information

• Chemical Name: octyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-D-arabinofuranoside
• CAS No.: 676259-68-0
• Molecular Formula: C₃₂H₅₆O₇Si₂
• Molecular Weight: 608.963
• Mol file: 676259-68-0.mol

Synonyms:octyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-D-arabinofuranoside

Chemical Property of octyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-D-arabinofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of octyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-D-arabinofuranoside

There total 1 articles about octyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane (69304-37-6) + benzoyl chloride (98-88-4) + octyl α-D-arabinofranose tetraacetate (352438-36-9) → octyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-D-arabinofuranoside (676259-68-0)

Guidance literature:

1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane; octyl α-D-arabinofranose tetraacetate; With pyridine; at 20 ℃; for 12h;

benzoyl chloride; at 20 ℃; Further stages.;

DOI:10.1016/j.tet.2003.12.022

Reference yield: 92.0%

octyl 2-O-benzoyl-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-D-arabinofuranoside (676259-68-0) → octyl 2-O-benzoyl-α-D-arabinofuranoside (310880-39-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1016/j.tet.2003.12.022

upstream raw materials:

1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

benzoyl chloride

octyl α-D-arabinofranose tetraacetate

Downstream raw materials:

octyl 2-O-benzoyl-α-D-arabinofuranoside