2-tert-butyl-1,3-((3-N-benzoyloxy-3-N-(2-trans-dodecenoyl))propyl)diamide citrate

Base Information

Chemical Name:2-tert-butyl-1,3-((3-N-benzoyloxy-3-N-(2-trans-dodecenoyl))propyl)diamide citrate
CAS No.:778591-27-8
Molecular Formula:C₅₄H₈₀N₄O₁₁
Molecular Weight:961.249
Hs Code.:

Synonyms:2-tert-butyl-1,3-((3-N-benzoyloxy-3-N-(2-trans-dodecenoyl))propyl)diamide citrate

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Chemical Property of 2-tert-butyl-1,3-((3-N-benzoyloxy-3-N-(2-trans-dodecenoyl))propyl)diamide citrate

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Technology Process of 2-tert-butyl-1,3-((3-N-benzoyloxy-3-N-(2-trans-dodecenoyl))propyl)diamide citrate

There total 4 articles about 2-tert-butyl-1,3-((3-N-benzoyloxy-3-N-(2-trans-dodecenoyl))propyl)diamide citrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 112767-08-5
2-trans-dodecenoyl chloride

: 778591-23-4
tert-butyl 4-((3-((benzoyloxy)amino)propyl)amino)-2-(2-((3-((benzoyloxy)amino)propyl)amino)-2-oxoethyl)-2-hydroxy-4-oxobutanoate

: 778591-27-8
2-tert-butyl-1,3-((3-N-benzoyloxy-3-N-(2-trans-dodecenoyl))propyl)diamide citrate

Guidance literature:: In dichloromethane; for 1h; Heating;
DOI:10.1021/ja048145j

Reference yield:

: 114340-53-3
2-tert-butyl-1,3-di-N-(hydroxyl) succinimidyl citrate

: 778591-27-8
2-tert-butyl-1,3-((3-N-benzoyloxy-3-N-(2-trans-dodecenoyl))propyl)diamide citrate

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / triethylamine / acetonitrile / 1 h / 25 °C

2: 78 percent / CH₂Cl₂ / 1 h / Heating

With triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/ja048145j

Reference yield:

: 198217-06-0
N^α-benzoyloxy-3-(tert-butoxycarbonylamino)propylamine

: 778591-27-8
2-tert-butyl-1,3-((3-N-benzoyloxy-3-N-(2-trans-dodecenoyl))propyl)diamide citrate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / HCl / diethyl ether; methanol / 1 h

2: 55 percent / triethylamine / acetonitrile / 1 h / 25 °C

3: 78 percent / CH₂Cl₂ / 1 h / Heating

With hydrogenchloride; triethylamine; In methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/ja048145j