TERT-BUTYL 6-AMINOPYRIDIN-2-YLCARBAMATE

Base Information

• Chemical Name: TERT-BUTYL 6-AMINOPYRIDIN-2-YLCARBAMATE
• CAS No.: 322690-31-3
• Molecular Formula: C10H15 N3 O2
• Molecular Weight: 209.248
• Hs Code.: 2933399090
• Mol file: 322690-31-3.mol

Synonyms:Carbamicacid, (6-amino-2-pyridinyl)-, 1,1-dimethylethyl ester (9CI);2-Amino-6-[(N-tert-butoxycarbonyl)amino]pyridine; tert-Butyl(6-aminopyridin-2-yl)carbamate

Chemical Property of TERT-BUTYL 6-AMINOPYRIDIN-2-YLCARBAMATE

Chemical Property:

• Vapor Pressure: 0.001mmHg at 25°C
• Melting Point: 125.0 to 129.0 °C
• Refractive Index: 1.587
• Boiling Point: 307.148°C at 760 mmHg
• PKA: 12.26±0.70(Predicted)
• Flash Point: 139.559°C
• PSA: 77.24000
• Density: 1.203g/cm³
• LogP: 2.66500
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C
• Solubility.: soluble in Methanol

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl6-Aminopyridin-2-ylcarbamate ^*data from reagent suppliers

Safty Information:

• Statements: 43
• Safety Statements: 36/37

MSDS Files:

SDS file from LookChem

Useful:

• Uses: tert-Butyl 6-Aminopyridin-2-ylcarbamate is used in preparation of novel Macrocyclic Diacetylene compounds.Also, used in preparation of substituted Bicyclic Aza-Heterocycles and analogs as Sirtuin modulators.

Technology Process of TERT-BUTYL 6-AMINOPYRIDIN-2-YLCARBAMATE

There total 1 articles about TERT-BUTYL 6-AMINOPYRIDIN-2-YLCARBAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2.6-diaminopyridine (141-86-6) + di-tert-butyl dicarbonate (24424-99-5) → (6-amino-pyridin-2-yl)-carbamic acid tert-butyl ester (322690-31-3)

Guidance literature:

In tetrahydrofuran; at 60 ℃;

DOI:10.1039/b809762c

Reference yield: 77.0%

(6-amino-pyridin-2-yl)-carbamic acid tert-butyl ester (322690-31-3) + terephthaloyl chloride (100-20-9) → C28H32N6O6

Guidance literature:

With triethylamine; In tetrahydrofuran;

DOI:10.3987/COM-06-10833

Reference yield: 60.0%

(6-amino-pyridin-2-yl)-carbamic acid tert-butyl ester (322690-31-3) + 3-(tritylthio) propanoic acid (27144-18-9) → C32H33N3O3S

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 45 ℃; for 12h; Inert atmosphere;

DOI:10.1002/chem.202101221

upstream raw materials:

2.6-diaminopyridine

di-tert-butyl dicarbonate

Downstream raw materials:

C₄₆H₄₆N₆O₈

C₂₃H₂₂N₄O₄S

C₂₄H₂₉N₅O₅

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