4-morpholine

Base Information

• Chemical Name: 4-morpholine
• CAS No.: 65407-88-7
• Molecular Formula: C₁₃H₁₆N₂O₃S
• Molecular Weight: 280.348

Synonyms:4-morpholine

Chemical Property of 4-morpholine

Chemical Property:

Purity/Quality:

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Technology Process of 4-morpholine

There total 7 articles about 4-morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

N-[1H-benzotriazol-1-yl(morpholino)methylidene]-4-methoxybenzamide → 4-morpholine (65407-88-7)

Guidance literature:

With hydrogen sulfide; In acetic acid; at 20 ℃; for 2h;

DOI:10.1055/s-2004-829127

Reference yield: 42.0%

4-methoxybenzoyl isothiocyanate (16778-84-0) + 1-(N-morpholino)cyclopent-1-ene (936-52-7) → cyclopentenopyrimidine-2,4-dithiol (16358-00-2) + 4-morpholine (65407-88-7) + [3-(4-Methoxy-benzoyl)-2,4-dithioxo-2,3,4,5,6,7-hexahydro-cyclopentapyrimidin-1-yl]-(4-methoxy-phenyl)-methanone (81268-77-1)

Guidance literature:

In chloroform; at 0 ℃; for 3h;

Reference yield: 30.0%

4-methoxybenzoyl isothiocyanate (16778-84-0) + 4-cyclohexen-1-ylmorpholine (670-80-4) → 4-morpholine (65407-88-7) + 2-(4-Methoxy-phenyl)-5,6,7,8-tetrahydro-benzo[e][1,3]oxazine-4-thione (81268-75-9) + cyclohexenopyrimidine-2,4-dithiol (16357-99-6)

Guidance literature:

In chloroform; 1.) 30 min, reflux, 2.) 1 day, room temperature;

upstream raw materials:

morpholine

ammonium thiocyanate

4-methoxy-benzoyl chloride

4-methoxybenzoyl isothiocyanate

Downstream raw materials:

N-[(aminocarbonyl)methyl]-4-methoxy-N'-[morpholino(thiocarbonyl)]benzamidine

2-(aminocarbonyl)-4-(4-methoxyphenyl)-6-morpholino-2H-1,3,5-thiadiazine

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