4-methoxy-N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]benzamidine

Base Information

Chemical Name:4-methoxy-N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]benzamidine
CAS No.:189452-42-4
Molecular Formula:C₁₆H₂₁N₃O₄S
Molecular Weight:351.426
Hs Code.:

Synonyms:4-methoxy-N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]benzamidine

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Chemical Property of 4-methoxy-N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]benzamidine

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Technology Process of 4-methoxy-N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]benzamidine

There total 2 articles about 4-methoxy-N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 189452-42-4
4-methoxy-N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]benzamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) MeCN, reflux, 2 h, 2.) MeCN, 30 min

2: 1.) SCCl₂, 2.) Et₃N / 1.) acetone, 15 min, 2.) MeCN, 10 min

With thiophosgene; triethylamine;
DOI:10.1021/jo970072h

Reference yield:

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 65407-88-7
4-morpholine

: 189452-42-4
4-methoxy-N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]benzamidine

Guidance literature:: With thiophosgene; triethylamine; Yield given. Multistep reaction; 1.) acetone, 15 min, 2.) MeCN, 10 min;
DOI:10.1021/jo970072h