benzyl 3,6-di-O-benzyl -2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

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Chemical Name:benzyl 3,6-di-O-benzyl -2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside
CAS No.:1443672-39-6
Molecular Formula:C₈₉H₉₄O₁₇
Molecular Weight:1435.72
Hs Code.:

Synonyms:benzyl 3,6-di-O-benzyl -2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

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Chemical Property of benzyl 3,6-di-O-benzyl -2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

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Technology Process of benzyl 3,6-di-O-benzyl -2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

There total 1 articles about benzyl 3,6-di-O-benzyl -2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1443672-38-5
benzyl 3-O-benzyl-2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

: 100-39-0
benzyl bromide

: 1443672-39-6
benzyl 3,6-di-O-benzyl -2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: benzyl 3-O-benzyl-2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside; With di(n-butyl)tin oxide; In toluene; for 3h; Reflux;

benzyl bromide; With cesium fluoride; In toluene; for 6h; regioselective reaction; Reflux;
DOI:10.1021/jo4005266

Reference yield: 80.0%

: 1443672-39-6
benzyl 3,6-di-O-benzyl -2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

: 2,3-di-O-benzyl-4,6-benzylidene-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2-O-benzoyl-3,6-di-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

: benzyl 2,3-Di-O-benzyl-4,6-benzylidene-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2-Obenzoyl-3,6-di-O-benzyl-β-D-glucopyranosyl-(1→4)-3,6-di-Obenzyl-2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: benzyl 3,6-di-O-benzyl -2-O-p-methoxybenzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside; 2,3-di-O-benzyl-4,6-benzylidene-β-D-mannopyranosyl-(1→4)-2,3,6-tri-O-benzyl-β-D-mannopyranosyl-(1→4)-2-O-benzoyl-3,6-di-O-benzyl-β-D-glucopyranosyl trichloroacetimidate; In toluene; Reflux;

In dichloromethane; toluene; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; toluene; at -78 - 0 ℃; for 6.5h;
DOI:10.1021/jo4005266