2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-(3-methyl-butyl) ester

Base Information

Chemical Name:2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-(3-methyl-butyl) ester
CAS No.:147597-20-4
Molecular Formula:C₂₃H₂₇N₃O₆
Molecular Weight:441.484
Hs Code.:

Synonyms:2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-(3-methyl-butyl) ester

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Chemical Property of 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-(3-methyl-butyl) ester

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Technology Process of 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-(3-methyl-butyl) ester

There total 3 articles about 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-(3-methyl-butyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.9%

: 193539-61-6
(Z)-3-Amino-but-2-enoic acid 2-cyano-ethyl ester

: 2-[1-(3-Nitro-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid 3-methyl-butyl ester

: 147597-20-4
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-(3-methyl-butyl) ester

Guidance literature:: In isopropyl alcohol; for 3h; Heating;
DOI:10.1248/cpb.41.108

Reference yield:

: 2308-18-1
isoamyl acetoacetate

: 147597-20-4
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-(3-methyl-butyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH, piperidine / benzene / 2 h / Heating

2: 74.9 percent / propan-2-ol / 3 h / Heating

With piperidine; acetic acid; In isopropyl alcohol; benzene;
DOI:10.1248/cpb.41.108

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 147597-20-4
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-(3-methyl-butyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH, piperidine / benzene / 2 h / Heating

2: 74.9 percent / propan-2-ol / 3 h / Heating

With piperidine; acetic acid; In isopropyl alcohol; benzene;
DOI:10.1248/cpb.41.108