N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

Base Information

Chemical Name:N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide
CAS No.:250261-54-2
Molecular Formula:C₂₉H₂₉NO₄Se
Molecular Weight:534.514
Hs Code.:

Synonyms:N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

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Chemical Property of N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

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Technology Process of N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

There total 6 articles about N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 5707-04-0
Phenylselenyl chloride

: 250261-53-1
N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)acetamide

: 250261-54-2
N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

Guidance literature:: N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)acetamide; With lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -78 ℃; for 0.75h;

Phenylselenyl chloride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -78 ℃; for 1h;
DOI:10.1039/a900467j

Reference yield:

: 2861-28-1
1,3-benzodioxole-5-acetic acid

: 250261-54-2
N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 94 percent / Et₃N / diethyl ether / 1 h / -78 - 0 °C

2.1: Pyridine / benzene / 2 h / 30 - 40 °C

3.1: LDA / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 0.75 h / -78 °C

3.2: 42 percent / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 1 h / -78 °C

With pyridine; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; hexane; benzene; 1.1: Substitution / 2.1: Acylation / 3.1: Metallation / 3.2: Substitution;
DOI:10.1039/a900467j

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 250261-54-2
N-(Cyclohex-1-enyl)-N-(4-methoxybenzyl)-2-(3,4-methylenedioxyphenyl)-2-(phenylseleno)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzene / 2 h / Heating

2.1: Pyridine / benzene / 2 h / 30 - 40 °C

3.1: LDA / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 0.75 h / -78 °C

3.2: 42 percent / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 1 h / -78 °C

With pyridine; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; benzene; 1.1: Condensation / 2.1: Acylation / 3.1: Metallation / 3.2: Substitution;
DOI:10.1039/a900467j