N-methyl-N-[6-(4-oxo-4H-1,3-benzothiazin-2-yl)-2-pyridyl]cyclohexanecarboxamide

Base Information

Chemical Name:N-methyl-N-[6-(4-oxo-4H-1,3-benzothiazin-2-yl)-2-pyridyl]cyclohexanecarboxamide
CAS No.:501375-90-2
Molecular Formula:C₂₁H₂₁N₃O₂S
Molecular Weight:379.483
Hs Code.:

Synonyms:N-methyl-N-[6-(4-oxo-4H-1,3-benzothiazin-2-yl)-2-pyridyl]cyclohexanecarboxamide

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Chemical Property of N-methyl-N-[6-(4-oxo-4H-1,3-benzothiazin-2-yl)-2-pyridyl]cyclohexanecarboxamide

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Technology Process of N-methyl-N-[6-(4-oxo-4H-1,3-benzothiazin-2-yl)-2-pyridyl]cyclohexanecarboxamide

There total 6 articles about N-methyl-N-[6-(4-oxo-4H-1,3-benzothiazin-2-yl)-2-pyridyl]cyclohexanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 501375-84-4
2-(6-Methylamino-2-pyridyl)-4H-1,3-benzothiazine-4-one

: 2719-27-9
cyclohexanylcarbonyl chloride

: 501375-90-2
N-methyl-N-[6-(4-oxo-4H-1,3-benzothiazin-2-yl)-2-pyridyl]cyclohexanecarboxamide

Guidance literature:: In N,N-dimethyl acetamide; at 80 ℃; for 2h;

Reference yield:

: tert-Butyl methyl(2-pyridyl)carbamate N-oxide

: 501375-90-2
N-methyl-N-[6-(4-oxo-4H-1,3-benzothiazin-2-yl)-2-pyridyl]cyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-Dimethylcarbamoyl chloride / Nitroethane / 48 h / 20 °C

2: triethylamine / toluene / 20 h / Heating / reflux

3: trifluoroacetic acid / 1 h / 20 °C

4: N,N-dimethyl acetamide / 2 h / 80 °C

With triethylamine; N,N-Dimethylcarbamoyl chloride; In Nitroethane; N,N-dimethyl acetamide; toluene; trifluoroacetic acid;

Reference yield:

: tert-Butyl 6-cyano-2-pyridylmethylcarbamate

: 501375-90-2
N-methyl-N-[6-(4-oxo-4H-1,3-benzothiazin-2-yl)-2-pyridyl]cyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / toluene / 20 h / Heating / reflux

2: trifluoroacetic acid / 1 h / 20 °C

3: N,N-dimethyl acetamide / 2 h / 80 °C

With triethylamine; In N,N-dimethyl acetamide; toluene; trifluoroacetic acid;