(2-amino-5-methylphenyl){1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amine

Base Information

Chemical Name:(2-amino-5-methylphenyl){1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amine
CAS No.:950771-79-6
Molecular Formula:C₂₀H₃₃N₃O
Molecular Weight:331.502
Hs Code.:

Synonyms:(2-amino-5-methylphenyl){1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amine

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Chemical Property of (2-amino-5-methylphenyl){1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amine

Chemical Property:

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Technology Process of (2-amino-5-methylphenyl){1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amine

There total 13 articles about (2-amino-5-methylphenyl){1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 950771-78-5
1-[trans-4-(ethyloxy)cyclohexyl]-N-(5-methyl-2-nitrophenyl)-4-piperidinamine

: 950771-79-6
(2-amino-5-methylphenyl){1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amine

Guidance literature:: With hydrazine; nickel; In ethanol; water; at 20 ℃; for 1h;

Reference yield:

: 3612-18-8
N-ethyl-4-piperidone

: 950771-79-6
(2-amino-5-methylphenyl){1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amine

Guidance literature:: Multi-step reaction with 5 steps

1: acetone / 3 h / 0 - 30 °C

2: potassium carbonate / ethanol; water / 80 °C

3: ammonia; hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2585.81 Torr

4: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24.5 h / 20 - 150 °C / Heating / reflux

5: hydrazine / nickel / ethanol; water / 1 h / 20 °C

With ammonia; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; hydrazine; palladium 10% on activated carbon; nickel; In methanol; ethanol; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: trans-4-hydroxycyclohexylamine hydrochloride

: 950771-79-6
(2-amino-5-methylphenyl){1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}amine

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / water / 3 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 - 40 °C

3: triethylsilane; bismuth(III) bromide / acetonitrile / 0 - 20 °C

4: hydrazine / methanol; ethanol / 3 h / Heating / reflux

5: potassium carbonate / ethanol; water / 80 °C

6: ammonia; hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2585.81 Torr

7: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24.5 h / 20 - 150 °C / Heating / reflux

8: hydrazine / nickel / ethanol; water / 1 h / 20 °C

With 1H-imidazole; triethylsilane; ammonia; hydrogen; bismuth(III) bromide; potassium carbonate; N-ethyl-N,N-diisopropylamine; hydrazine; palladium 10% on activated carbon; nickel; In methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;