(((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate)

Base Information

Chemical Name:(((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate)
CAS No.:1610375-33-1
Molecular Formula:C₃₁H₄₁N₂O₁₂P
Molecular Weight:664.646
Hs Code.:

(((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate)

Synonyms:(((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate)

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Chemical Property of (((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate)

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Technology Process of (((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate)

There total 4 articles about (((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 53064-79-2
iodomethyl pivaloate

: 1610375-32-0
benzyl 2-(dimethoxyphosphoryl)-2-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)acetate

: 1610375-33-1
(((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate)

Guidance literature:: benzyl 2-(dimethoxyphosphoryl)-2-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)acetate; With 2,6-dimethylpyridine; trimethylsilyl bromide; In acetonitrile; at 50 ℃; for 0.166667h; Microwave irradiation;

With methanol; In water; acetonitrile; at 20 ℃; for 0.166667h;

iodomethyl pivaloate; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile; at 20 ℃;

Reference yield:

: 57443-18-2
benzyl 2-(dimethoxyphosphoryl)acetate

: 1610375-33-1
(((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; dodecylbenzenesulfonyl azide / acetonitrile / 20 - 40 °C

2.1: benzene / 0.03 h / Inert atmosphere; Molecular sieve

2.2: 24 h / Reflux; Inert atmosphere

3.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 2 h / 50 °C / Microwave irradiation; Inert atmosphere

4.1: 2,6-dimethylpyridine; trimethylsilyl bromide / acetonitrile / 0.17 h / 50 °C / Microwave irradiation

4.2: 0.17 h / 20 °C

4.3: 20 °C

With 2,6-dimethylpyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dodecylbenzenesulfonyl azide; trimethylsilyl bromide; sodium carbonate; triethylamine; In acetonitrile; benzene;

Reference yield:

: 1610375-30-8
benzyl (dimethylphosphono)diazoacetate

: 1610375-33-1
(((2-(benzyloxy)-1-(((1S,4R)-4-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopent-2-en-1-yl)oxy)-2-oxoethyl)phosphoryl)bis(oxy))bis(methylene) bis(2,2-dimethylpropanoate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzene / 0.03 h / Inert atmosphere; Molecular sieve

1.2: 24 h / Reflux; Inert atmosphere

2.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 2 h / 50 °C / Microwave irradiation; Inert atmosphere

3.1: 2,6-dimethylpyridine; trimethylsilyl bromide / acetonitrile / 0.17 h / 50 °C / Microwave irradiation

3.2: 0.17 h / 20 °C

3.3: 20 °C

With 2,6-dimethylpyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trimethylsilyl bromide; sodium carbonate; In acetonitrile; benzene;