1-phenylthio-2-trifluoroacetoxyoctane

Base Information

• Chemical Name: 1-phenylthio-2-trifluoroacetoxyoctane
• CAS No.: 80437-03-2
• Molecular Formula: C₁₆H₂₁F₃O₂S
• Molecular Weight: 334.403

Synonyms:1-phenylthio-2-trifluoroacetoxyoctane

Chemical Property of 1-phenylthio-2-trifluoroacetoxyoctane

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1-phenylthio-2-trifluoroacetoxyoctane

There total 3 articles about 1-phenylthio-2-trifluoroacetoxyoctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

oct-1-ene (111-66-0,25068-25-1) + S-phenyl benzenethiosulfinate (1208-20-4,6930-77-4,133670-27-6) + trifluoroacetic anhydride (407-25-0) → 1-phenylthio-2-trifluoroacetoxyoctane (80437-03-2)

Guidance literature:

In tetrachloromethane; at -20 ℃;

DOI:10.1016/S0040-4020(01)98953-7

Reference yield:

oct-1-ene (111-66-0,25068-25-1) + diphenyldisulfane (882-33-7) + trifluoroacetic acid (76-05-1) → 1-phenylthio-2-trifluoroacetoxyoctane (80437-03-2)

Guidance literature:

With manganese triacetate; In dichloromethane; at 0 ℃; for 0.5h; Yield given;

DOI:10.1039/P19850001039

Reference yield:

oct-1-ene (111-66-0,25068-25-1) + S-phenyl benzenethiosulfinate (1208-20-4,6930-77-4,133670-27-6) + trifluoroacetic anhydride (407-25-0) → 1,2-bis(phenylthio)octane + 1-phenylthio-2-trifluoroacetoxyoctane (80437-03-2)

Guidance literature:

In tetrachloromethane; at -20 ℃;

DOI:10.1016/S0040-4020(01)98953-7

upstream raw materials:

oct-1-ene

diphenyldisulfane

trifluoroacetic acid

S-phenyl benzenethiosulfinate

Downstream raw materials:

1-(phenylthio)octan-2-ol

2-acetamido-1-phenylthio-octane

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