tert-butyl ({[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl}oxy)(2-nitrophenyl)acetate

Base Information

Chemical Name:tert-butyl ({[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl}oxy)(2-nitrophenyl)acetate
CAS No.:1345834-27-6
Molecular Formula:C₁₇H₁₈N₂O₉
Molecular Weight:394.338
Hs Code.:

Synonyms:tert-butyl ({[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl}oxy)(2-nitrophenyl)acetate

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Chemical Property of tert-butyl ({[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl}oxy)(2-nitrophenyl)acetate

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Technology Process of tert-butyl ({[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl}oxy)(2-nitrophenyl)acetate

There total 4 articles about tert-butyl ({[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl}oxy)(2-nitrophenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 74124-79-1
di(succinimido) carbonate

: 191476-01-4
t-butyl 2-hydroxy-2-[2-nitrophenyl]acetate

: 1345834-27-6
tert-butyl ({[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl}oxy)(2-nitrophenyl)acetate

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1039/c1cc13355a

Reference yield:

: 13312-81-7
2-hydroxy-2-[2-nitrophenyl]acetonitrile

: 1345834-27-6
tert-butyl ({[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl}oxy)(2-nitrophenyl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride; water / 6 h / Reflux

2: 1 h / Reflux

3: toluene / 1 h

4: methanol; caesium carbonate / 1 h / 65 °C

5: triethylamine / acetonitrile / 8 h / 20 °C / Inert atmosphere

With hydrogenchloride; methanol; water; caesium carbonate; triethylamine; In toluene; acetonitrile;
DOI:10.1039/c1cc13355a

Reference yield:

: 103262-47-1
2-acetoxy-2-[2-nitrophenyl]acetic acid

: 1345834-27-6
tert-butyl ({[(2,5-dioxo-1-pyrrolidinyl)oxy]carbonyl}oxy)(2-nitrophenyl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 1 h

2: methanol; caesium carbonate / 1 h / 65 °C

3: triethylamine / acetonitrile / 8 h / 20 °C / Inert atmosphere

With methanol; caesium carbonate; triethylamine; In toluene; acetonitrile;
DOI:10.1039/c1cc13355a