1-[(2S,3S)-3-{N₂-[4-(benzyloxycarbonylamino)phenoxyacetyl]-L-asparaginyl}amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide

Base Information

• Chemical Name: 1-[(2S,3S)-3-{N₂-[4-(benzyloxycarbonylamino)phenoxyacetyl]-L-asparaginyl}amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide
• CAS No.: 166382-76-9
• Molecular Formula: C₃₉H₄₈N₆O₉
• Molecular Weight: 744.845

Synonyms:1-[(2S,3S)-3-{N₂-[4-(benzyloxycarbonylamino)phenoxyacetyl]-L-asparaginyl}amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide

Chemical Property of 1-[(2S,3S)-3-{N₂-[4-(benzyloxycarbonylamino)phenoxyacetyl]-L-asparaginyl}amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide

Chemical Property:

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Technology Process of 1-[(2S,3S)-3-{N₂-[4-(benzyloxycarbonylamino)phenoxyacetyl]-L-asparaginyl}amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide

There total 1 articles about 1-[(2S,3S)-3-{N₂-[4-(benzyloxycarbonylamino)phenoxyacetyl]-L-asparaginyl}amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-benzyloxycarbonylaminophenoxy)acetic acid (166383-74-0) + 1-[(2S,3S)-3-(L-asparaginylamino)-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide hydrochloride (145064-75-1) → 1-[(2S,3S)-3-{N2-[4-(benzyloxycarbonylamino)phenoxyacetyl]-L-asparaginyl}amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide (166382-76-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane;

Reference yield:

1-[(2S,3S)-3-{N2-[4-(benzyloxycarbonylamino)phenoxyacetyl]-L-asparaginyl}amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide (166382-76-9) → 1-{(2S,3S)-3-[N2-(4-Aminophenoxyacetyl)-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide hydrochloride (166382-77-0)

Guidance literature:

With hydrogenchloride; In methanol; palladium;

upstream raw materials:

2-(4-benzyloxycarbonylaminophenoxy)acetic acid

1-[(2S,3S)-3-(L-asparaginylamino)-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide hydrochloride

Downstream raw materials:

1-{(2S,3S)-3-[N₂-(4-Aminophenoxyacetyl)-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide hydrochloride

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