N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)picolinethioamide

Base Information

Chemical Name:N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)picolinethioamide
CAS No.:1403990-60-2
Molecular Formula:C₂₅H₁₇N₅OS
Molecular Weight:435.509
Hs Code.:

Synonyms:N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)picolinethioamide

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Chemical Property of N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)picolinethioamide

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Technology Process of N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)picolinethioamide

There total 2 articles about N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)picolinethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1403990-54-4
N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)picolinamide

: 1403990-61-3
1,3-diphenyl-7-pyridin-2-yl-1,4-dihydrothiazolo[5',4':4,5]benzo[1,2-e][1,2,4]-triazin-4-yl

: 1403990-60-2
N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)picolinethioamide

Guidance literature:: With tetraphosphorus decasulfide; In toluene; at 110 ℃; for 0.5h;
DOI:10.1021/ol302714j

Reference yield:

: 22751-79-7
1,3-diphenylbenzo[e]-[1,2,4]triazin-7(1H)-one

: 1403990-60-2
N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)picolinethioamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: O-benzylhydoxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 1 h / 20 - 78 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C

2.2: 12 h / 20 °C

3.1: tetraphosphorus decasulfide / toluene / 0.5 h / 110 °C

With tetraphosphorus decasulfide; O-benzylhydoxylamine hydrochloride; sodium hydride; N-ethyl-N,N-diisopropylamine; In ethanol; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ol302714j