Trifluoro-methanesulfinic acid benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amide

Base Information

Chemical Name:Trifluoro-methanesulfinic acid benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amide
CAS No.:848572-70-3
Molecular Formula:C₂₅H₂₈F₃NO₂SSi
Molecular Weight:491.65
Hs Code.:

Synonyms:Trifluoro-methanesulfinic acid benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amide

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Chemical Property of Trifluoro-methanesulfinic acid benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amide

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Technology Process of Trifluoro-methanesulfinic acid benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amide

There total 2 articles about Trifluoro-methanesulfinic acid benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amine

: 41804-89-1
potassium triflinate

: 848572-70-3
Trifluoro-methanesulfinic acid benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amide

Guidance literature:: potassium triflinate; With trichlorophosphate; In dichloromethane; at 20 ℃; for 0.666667h;

Benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/chem.200400777

Reference yield:

: 153322-12-4
(1S,2R)-2-(N-benzylamino)-1,2-diphenylethanol

: 848572-70-3
Trifluoro-methanesulfinic acid benzyl-((1R,2S)-1,2-diphenyl-2-trimethylsilanyloxy-ethyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: CH₂Cl₂ / 0 - 20 °C

2.1: POCl₃ / CH₂Cl₂ / 0.67 h / 20 °C

2.2: diisopropylethylamine / CH₂Cl₂ / 0 - 20 °C

With trichlorophosphate; In dichloromethane;
DOI:10.1002/chem.200400777