2,5-Bis-allyloxy-N,N'-bis-((S)-1-chloromethyl-2-methyl-propyl)-terephthalamide

Base Information

Chemical Name:2,5-Bis-allyloxy-N,N'-bis-((S)-1-chloromethyl-2-methyl-propyl)-terephthalamide
CAS No.:214205-97-7
Molecular Formula:C₂₄H₃₄Cl₂N₂O₄
Molecular Weight:485.451
Hs Code.:

Synonyms:2,5-Bis-allyloxy-N,N'-bis-((S)-1-chloromethyl-2-methyl-propyl)-terephthalamide

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Chemical Property of 2,5-Bis-allyloxy-N,N'-bis-((S)-1-chloromethyl-2-methyl-propyl)-terephthalamide

Chemical Property:

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Technology Process of 2,5-Bis-allyloxy-N,N'-bis-((S)-1-chloromethyl-2-methyl-propyl)-terephthalamide

There total 4 articles about 2,5-Bis-allyloxy-N,N'-bis-((S)-1-chloromethyl-2-methyl-propyl)-terephthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5870-38-2
diethyl 2,5-(dihydroxy)terephthalate

: 214205-97-7
2,5-Bis-allyloxy-N,N'-bis-((S)-1-chloromethyl-2-methyl-propyl)-terephthalamide

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / K₂CO₃ / dimethylformamide / 13 h / Ambient temperature

2: 96 percent / aq. LiOH / tetrahydrofuran / 5 h / Heating

3: SOCl₂ / 3 h / Heating

4: Et₃N / CH₂Cl₂ / 12 h / Ambient temperature

5: 93 percent / SOCl₂ / CH₂Cl₂ / 17 h

With lithium hydroxide; thionyl chloride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo980561x

Reference yield:

: 149590-60-3
2,5-bis(allyloxy)-1,4-benzenedicarboxylic acid

: 214205-97-7
2,5-Bis-allyloxy-N,N'-bis-((S)-1-chloromethyl-2-methyl-propyl)-terephthalamide

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 3 h / Heating

2: Et₃N / CH₂Cl₂ / 12 h / Ambient temperature

3: 93 percent / SOCl₂ / CH₂Cl₂ / 17 h

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo980561x

Reference yield:

: 149590-59-0
diethyl 2,5-bis(allyloxy)terephthalate

: 214205-97-7
2,5-Bis-allyloxy-N,N'-bis-((S)-1-chloromethyl-2-methyl-propyl)-terephthalamide

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / aq. LiOH / tetrahydrofuran / 5 h / Heating

2: SOCl₂ / 3 h / Heating

3: Et₃N / CH₂Cl₂ / 12 h / Ambient temperature

4: 93 percent / SOCl₂ / CH₂Cl₂ / 17 h

With lithium hydroxide; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo980561x