C₄₇H₇₂F₂O₅SSi

Base Information

Chemical Name:C₄₇H₇₂F₂O₅SSi
CAS No.:1338560-82-9
Molecular Formula:C₄₇H₇₂F₂O₅SSi
Molecular Weight:815.234
Hs Code.:

C<sub>47</sub>H<sub>72</sub>F<sub>2</sub>O<sub>5</sub>SSi

Synonyms:C₄₇H₇₂F₂O₅SSi

Suppliers and Price of C₄₇H₇₂F₂O₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₇₂F₂O₅SSi

Chemical Property:

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Technology Process of C₄₇H₇₂F₂O₅SSi

There total 3 articles about C₄₇H₇₂F₂O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1338560-78-3
C₁₆H₁₇F₂IO₂S

: 685091-63-8
(8R,9R,12R,13R)-13-(tert-butyldimethylsilyloxy)-9,12-epoxy-pentacosa-1,6-diyn-8-ol

: 1338560-82-9
C₄₇H₇₂F₂O₅SSi

Guidance literature:: With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine; at 20 ℃;
DOI:10.1016/j.bmcl.2011.08.011

Reference yield:

: 1338560-77-2
C₁₈H₂₈F₂O₃SSi

: 1338560-82-9
C₄₇H₇₂F₂O₅SSi

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / Reflux

2: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C

3: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; toluene-4-sulfonic acid; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; toluene; 3: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.08.011

Reference yield:

: 1338560-69-2
C₁₁H₁₀F₂O₂S

: 1338560-82-9
C₄₇H₇₂F₂O₅SSi

Guidance literature:: Multi-step reaction with 2 steps

1: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C

2: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; 2: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.08.011