C₆₀H₇₀N₈O₁₃Si

Base Information

Chemical Name:C₆₀H₇₀N₈O₁₃Si
CAS No.:1287721-55-4
Molecular Formula:C₆₀H₇₀N₈O₁₃Si
Molecular Weight:1139.35
Hs Code.:

C<sub>60</sub>H<sub>70</sub>N<sub>8</sub>O<sub>13</sub>Si

Synonyms:C₆₀H₇₀N₈O₁₃Si

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Chemical Property of C₆₀H₇₀N₈O₁₃Si

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Technology Process of C₆₀H₇₀N₈O₁₃Si

There total 10 articles about C₆₀H₇₀N₈O₁₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1287721-54-3
5'-amino-N₆-benzoyl-5'-deoxy-2'-O-(triisopropylsilyloxymethyl)adenosine

: 1287721-52-1
C₃₃H₃₂N₂O₉

: 1287721-55-4
C₆₀H₇₀N₈O₁₃Si

Guidance literature:: With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201007012

Reference yield:

: 1287721-51-0
1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil

: 1287721-55-4
C₆₀H₇₀N₈O₁₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: sodium dihydrogenphosphate; sodium chlorite; water / dimethyl sulfoxide; tert-butyl alcohol / 30 h / 20 °C / Inert atmosphere

2: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; acetonitrile / 12 h / 20 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; water; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; dimethyl sulfoxide; acetonitrile; tert-butyl alcohol;
DOI:10.1002/anie.201007012

Reference yield:

: 1287721-53-2
5'-azido-N₆-benzoyl-5'-deoxy-2'-O-(triisopropylsilyloxymethyl)adenosine

: 1287721-55-4
C₆₀H₇₀N₈O₁₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 14 h / 20 °C

2: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; acetonitrile / 12 h / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1002/anie.201007012