6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)-3-pyridinecarboxylic acid

Base Information

• Chemical Name: 6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)-3-pyridinecarboxylic acid
• CAS No.: 171002-75-8
• Molecular Formula: C₁₈H₂₀N₂O₄
• Molecular Weight: 328.368

Synonyms:6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)-3-pyridinecarboxylic acid

Chemical Property of 6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)-3-pyridinecarboxylic acid

Chemical Property:

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Technology Process of 6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)-3-pyridinecarboxylic acid

There total 1 articles about 6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)-3-pyridinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N-<3-<6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)pyridinecarbonyl>>-N-methyl carbamic acid (1,1-dimethylethyl) ester → 6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)-3-pyridinecarboxylic acid (171002-75-8)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; for 24h; Ambient temperature;

DOI:10.1016/0040-4020(95)00596-Z

Reference yield: 91.0%

6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)-3-pyridinecarboxylic acid (171002-75-8) → 6--4-(6-bromo-3-methoxyphenyl)-3-pyridinecarboxylic acid (171002-82-7)

Guidance literature:

With hexamethylene tetramine hydrobromide perbromide; In methanol; dichloromethane; Ambient temperature;

DOI:10.1016/0040-4020(95)00596-Z

Reference yield: 81.0%

6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)-3-pyridinecarboxylic acid (171002-75-8) + tert-butyl alcohol (75-65-0) → 3-<6-<(1,1-dimethylethylamino)carbonyl>-4-(3-methoxyphenyl)pyridinyl>carbamic acid (1,1-dimethylethyl) ester

Guidance literature:

With diphenyl-phosphinic acid; triethylamine; 1 h, RT; reflux, 16 h;

DOI:10.1016/0040-4020(95)00596-Z

Downstream raw materials:

6--4-(6-bromo-3-methoxyphenyl)-3-pyridinecarboxylic acid

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