ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate

Base Information

Chemical Name:ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate
CAS No.:919082-36-3
Molecular Formula:C₅₂H₄₉NO₉
Molecular Weight:831.962
Hs Code.:

ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate

Synonyms:ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate

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Chemical Property of ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate

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Technology Process of ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate

There total 21 articles about ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 478855-43-5
6-benzyloxy-1-(3,4-dimethoxy-benzyl)-7-methoxy-3,4-dihydro-isoquinoline

: 1034028-91-5
(Z)-ethyl 2,4-bis(benzyloxy)-5-methoxy-α-nitrocinnamate

: 919082-36-3
ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate

Guidance literature:: With sodium hydrogencarbonate; In acetonitrile; for 18h; Heating;
DOI:10.1021/jo061810h

Reference yield: 61.0%

: ethyl 8-(benzyloxy)-2-(2,5-bis(benzyloxy)-4-methoxyphenyl)-1-bromo-9-methoxy-5,6-dihydropyrrolo[2,1-a]isoquinoline-3-carboxylate

: 365564-10-9
2-(3,4-dimethoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 919082-36-3
ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; barium hydroxide octahydrate; In 1,4-dioxane; at 100 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/acs.joc.1c01505

Reference yield:

: 100-39-0
benzyl bromide

: 919082-36-3
ethyl 8-(benzyloxy)-2-(2,4-bis(benzyloxy)-5-methoxyphenyl)-1-(3,4-dimethoxyphenyl)-9-methoxy-5,6-dihydropyrrolo[2,1-a]-isoquinoline-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: sodium hydrogencarbonate / acetonitrile / 18 h / Heating

With sodium hydrogencarbonate; In acetonitrile;
DOI:10.1021/jo061810h