3-hydroxy-3-methylthiazolo<1,2-b>indol-9-yltriphenylphosphonium bromide

Base Information

Chemical Name:3-hydroxy-3-methylthiazolo<1,2-b>indol-9-yltriphenylphosphonium bromide
CAS No.:115134-69-5
Molecular Formula:Br*C₂₉H₂₅NOPS
Molecular Weight:546.467
Hs Code.:

Synonyms:3-hydroxy-3-methylthiazolo<1,2-b>indol-9-yltriphenylphosphonium bromide

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Chemical Property of 3-hydroxy-3-methylthiazolo<1,2-b>indol-9-yltriphenylphosphonium bromide

Chemical Property:

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Technology Process of 3-hydroxy-3-methylthiazolo<1,2-b>indol-9-yltriphenylphosphonium bromide

There total 4 articles about 3-hydroxy-3-methylthiazolo<1,2-b>indol-9-yltriphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 3-triphenylphosphoniumindolyl-2-thiolate

: 598-31-2
1-bromoacetone

: 115134-69-5
3-hydroxy-3-methylthiazolo<1,2-b>indol-9-yltriphenylphosphonium bromide

Guidance literature:: In ethanol; at 15 ℃; for 4h;

Reference yield:

: 115134-61-7
2-isothiocyanatobenzyltriphenylphosphonium bromide

: 115134-69-5
3-hydroxy-3-methylthiazolo<1,2-b>indol-9-yltriphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / triethylamine / acetonitrile / 1 h

2: 97 percent / ethanol / 4 h / 15 °C

With triethylamine; In ethanol; acetonitrile;

Reference yield:

: 108288-40-0
2-(bromomethyl)phenyl isothiocyanate

: 115134-69-5
3-hydroxy-3-methylthiazolo<1,2-b>indol-9-yltriphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / diethyl ether / 1 h / Heating

2: 94 percent / triethylamine / acetonitrile / 1 h

3: 97 percent / ethanol / 4 h / 15 °C

With triethylamine; In diethyl ether; ethanol; acetonitrile;