1H-Imidazole, 5-[(4-methyl-3-cyclohexen-1-yl)methyl]-

Base Information

Chemical Name:1H-Imidazole, 5-[(4-methyl-3-cyclohexen-1-yl)methyl]-
CAS No.:317338-02-6
Molecular Formula:C11H16 N2
Molecular Weight:176.26
Hs Code.:
Mol file:317338-02-6.mol

Synonyms:1H-Imidazole,4-[(4-methyl-3-cyclohexen-1-yl)methyl]- (9CI)

Suppliers and Price of 1H-Imidazole, 5-[(4-methyl-3-cyclohexen-1-yl)methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1H-Imidazole, 5-[(4-methyl-3-cyclohexen-1-yl)methyl]-

Chemical Property:

PSA：28.68000
LogP:2.69860

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Imidazole, 5-[(4-methyl-3-cyclohexen-1-yl)methyl]-

There total 8 articles about 1H-Imidazole, 5-[(4-methyl-3-cyclohexen-1-yl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 628731-68-0
C₁₃H₂₁N₃O₂S

: 628731-70-4
C₁₃H₂₁N₃O₂S

: 317338-02-6
C₁₁H₁₆N₂

: 317338-58-2
C₁₁H₁₆N₂

Guidance literature:: With potassium hydroxide; Celite; In methanol; water; for 30h; Heating / reflux;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 317338-02-6
C₁₁H₁₆N₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / tetrahydrofuran / 18.5 h / 0 - 20 °C

2.1: Celite; hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

3.1: lithium aluminium tetrahydride; Celite / tetrahydrofuran / 1 h / -78 - 20 °C

4.1: oxalyl dichloride; Celite; dimethyl sulfoxide; triethylamine / dichloromethane / 2.5 h / -78 - 20 °C

5.1: Celite; sodium cyanide; dimethyl sulfoxide; triethylamine / ethanol / 5 h / 20 °C

5.2: 3.5 h / 100 °C

6.1: hydrogenchloride; Celite / acetone / 5 h

7.1: Celite; triethylamine / DMF (N,N-dimethyl-formamide) / 16 h

8.1: Celite / tetrahydrofuran / 16 h

9.1: Burgess Reagent; Celite / benzene / 1 h / 20 °C

10.1: potassium hydroxide; Celite / methanol; water / 30 h / Heating / reflux

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; Burgess Reagent; Celite; sodium cyanide; hydrogen; sodium hydride; dimethyl sulfoxide; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; ethyl acetate; acetone; benzene;

Reference yield:

: 172270-85-8
8-(methoxyformylmethylene)-1,4-dioxaspiro[4.5]decane

: 317338-02-6
C₁₁H₁₆N₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: Celite; hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

2.1: lithium aluminium tetrahydride; Celite / tetrahydrofuran / 1 h / -78 - 20 °C

3.1: oxalyl dichloride; Celite; dimethyl sulfoxide; triethylamine / dichloromethane / 2.5 h / -78 - 20 °C

4.1: Celite; sodium cyanide; dimethyl sulfoxide; triethylamine / ethanol / 5 h / 20 °C

4.2: 3.5 h / 100 °C

5.1: hydrogenchloride; Celite / acetone / 5 h

6.1: Celite; triethylamine / DMF (N,N-dimethyl-formamide) / 16 h

7.1: Celite / tetrahydrofuran / 16 h

8.1: Burgess Reagent; Celite / benzene / 1 h / 20 °C

9.1: potassium hydroxide; Celite / methanol; water / 30 h / Heating / reflux

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; Burgess Reagent; Celite; sodium cyanide; hydrogen; dimethyl sulfoxide; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; ethyl acetate; acetone; benzene;