METHYL-4-BROMOMETHYLPYRIDINE-2-CARBOXYLATE

Base Information

Chemical Name:METHYL-4-BROMOMETHYLPYRIDINE-2-CARBOXYLATE
CAS No.:317335-16-3
Molecular Formula:C8H8 Br N O2
Molecular Weight:230.061
Hs Code.:2933399090
Mol file:317335-16-3.mol

Synonyms:Methyl4-(bromomethyl)pyridine-2-carboxylate

Suppliers and Price of METHYL-4-BROMOMETHYLPYRIDINE-2-CARBOXYLATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Methyl4-(bromomethyl)picolinate 95+%
1g
$ 982.00

Chemenu
Methyl4-(bromomethyl)picolinate 95%
1g
$ 926.00

American Custom Chemicals Corporation
METHYL-4-BROMOMETHYLPYRIDINE-2-CARBOXYLATE 95.00%
1G
$ 1794.87

American Custom Chemicals Corporation
METHYL-4-BROMOMETHYLPYRIDINE-2-CARBOXYLATE 95.00%
500MG
$ 1370.41

Abosyn
Methyl-4-bromomethylpyridine-2-carboxylate 95%-98%
1g
$ 1200.00

Total 13 raw suppliers

Chemical Property of METHYL-4-BROMOMETHYLPYRIDINE-2-CARBOXYLATE

Chemical Property:

Vapor Pressure:0.000108mmHg at 25°C
Melting Point:0°C
Refractive Index:1.563
Boiling Point:0°C
Flash Point:157.6°C
PSA：39.19000
Density:1.533g/cm³
LogP:1.76310
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Methyl4-(bromomethyl)picolinate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of METHYL-4-BROMOMETHYLPYRIDINE-2-CARBOXYLATE

There total 7 articles about METHYL-4-BROMOMETHYLPYRIDINE-2-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 13509-13-2
4-methylpyridine-2-carboxylic acid methyl ester

: 317335-16-3
methyl 4-(bromomethyl)picolinate

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 80 ℃; for 4h;

Reference yield:

: 317335-15-2
methyl 4-(hydroxymethyl)pyridine-2-carboxylate

: 317335-16-3
methyl 4-(bromomethyl)picolinate

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃;

Reference yield:

: 586-95-8
pyridine-4-methanol

: 317335-16-3
methyl 4-(bromomethyl)picolinate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / DMF (N,N-dimethyl-formamide) / 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

3.1: N,N-Dimethylcarbamoyl chloride / dichloromethane / 0 - 20 °C

3.2: 0.5 h

4.1: hydrogenchloride; water / 5 h / Heating / reflux

5.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 20 °C

With 1H-imidazole; hydrogenchloride; carbon tetrabromide; water; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; N,N-Dimethylcarbamoyl chloride; In DMF (N,N-dimethyl-formamide); dichloromethane;