cyclohexyl 2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Base Information

• Chemical Name: cyclohexyl 2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside
• CAS No.: 908577-23-1
• Molecular Formula: C₃₂H₄₆O₁₈
• Molecular Weight: 718.706

Synonyms:cyclohexyl 2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Chemical Property of cyclohexyl 2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of cyclohexyl 2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

There total 2 articles about cyclohexyl 2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-O-(2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl trichloracetimidate (92052-38-5,106256-81-9,106256-89-7,126736-02-5,132287-70-8,132287-71-9,139403-73-9,130703-21-8) + cyclohexanol (108-93-0) → cyclohexyl 2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside (908577-23-1)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at -18 - 20 ℃; Inert atmosphere; Molecular sieve;

DOI:10.1021/ja805147t

Reference yield:

acetobromocellobiose (14227-66-8) + cyclohexanol (108-93-0) → cyclohexyl 2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside (908577-23-1)

Guidance literature:

With mercury(II) diacetate; aluminium; benzene;

Reference yield: 99.0%

cyclohexyl 2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside (908577-23-1) → cyclohexyl β-D-glucopyranosyl-(1->4)-α-D-glucopyranoside (793668-61-8)

Guidance literature:

With sodium methylate; In methanol; dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja805147t

upstream raw materials:

acetobromocellobiose

cyclohexanol

4-O-(2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl trichloracetimidate

Downstream raw materials:

cyclohexyl β-D-glucopyranosyl-(1->4)-α-D-glucopyranoside

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