methyl 3'-{[(1S)-1-cyclohexylethyl](methyl)carbamoyl}-2,2'-binaphthalene-3-carboxylate

Base Information

Chemical Name:methyl 3'-{[(1S)-1-cyclohexylethyl](methyl)carbamoyl}-2,2'-binaphthalene-3-carboxylate
CAS No.:906560-77-8
Molecular Formula:C₃₂H₃₃NO₃
Molecular Weight:479.619
Hs Code.:

Synonyms:methyl 3'-{[(1S)-1-cyclohexylethyl](methyl)carbamoyl}-2,2'-binaphthalene-3-carboxylate

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Chemical Property of methyl 3'-{[(1S)-1-cyclohexylethyl](methyl)carbamoyl}-2,2'-binaphthalene-3-carboxylate

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Technology Process of methyl 3'-{[(1S)-1-cyclohexylethyl](methyl)carbamoyl}-2,2'-binaphthalene-3-carboxylate

There total 4 articles about methyl 3'-{[(1S)-1-cyclohexylethyl](methyl)carbamoyl}-2,2'-binaphthalene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 906560-69-8
methyl 3'-([(1S)-1-cyclohexylethyl]carbamoyl)-2,2'-binaphthalene-3-carboxylate

: 74-88-4
methyl iodide

: 906560-77-8
methyl 3'-{[(1S)-1-cyclohexylethyl](methyl)carbamoyl}-2,2'-binaphthalene-3-carboxylate

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.06.013

Reference yield:

: 106653-99-0
3'-(methoxycarbonyl)-2,2'-binaphthalene-3-carboxylic acid

: 906560-77-8
methyl 3'-{[(1S)-1-cyclohexylethyl](methyl)carbamoyl}-2,2'-binaphthalene-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; thionyl chloride / dichloromethane / 2 h / 10 °C / Inert atmosphere

2: zinc(II) iodide / dichloromethane / 3 h / 10 - 20 °C / Inert atmosphere

3: acetonitrile / 20 °C / Inert atmosphere

4: sodium hydride / dimethyl sulfoxide / 24 h / 20 °C / Inert atmosphere

With pyridine; thionyl chloride; sodium hydride; zinc(II) iodide; In dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.tetasy.2012.06.013

Reference yield:

: 386707-15-9
methyl 3'-(cyanocarbonyl)-2,2'-binaphthalene-3-carboxylate

: 906560-77-8
methyl 3'-{[(1S)-1-cyclohexylethyl](methyl)carbamoyl}-2,2'-binaphthalene-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 20 °C / Inert atmosphere

2: sodium hydride / dimethyl sulfoxide / 24 h / 20 °C / Inert atmosphere

With sodium hydride; In dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.tetasy.2012.06.013