1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene

Base Information

Chemical Name:1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene
CAS No.:863514-01-6
Molecular Formula:C₂₅H₃₁N₃
Molecular Weight:373.541
Hs Code.:

Synonyms:1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene

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Chemical Property of 1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene

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Technology Process of 1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene

There total 1 articles about 1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1821-47-2
5-methyltryptamine

: 65619-20-7
4-dimethylamino-4-phenylcyclohexanone

: 863514-01-6
1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene

Guidance literature:: 5-methyltryptamine; 4-dimethylamino-4-phenylcyclohexanone; With sodium sulfate; In methanol; for 24h;

With trifluoroacetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 18h;

With sodium hydroxide; In water; pH=11;

Reference yield:

: 863514-01-6
1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene

: 108-24-7
acetic anhydride

: 2-acetyl-1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene

Guidance literature:: 1,1-(3-dimethylamino-3-phenyl-pentamethylen)-6-methyl-3,4-dihydro-1H-2,9-diazafluorene; acetic anhydride; With pyridine; at 20 ℃; for 72h;

With sodium hydroxide; In water; pH=11;