methyl N-[3-(4-nitrophenyl)-2,2-trimethylenedithiopropionyl]-L-phenylalaninate

Base Information

Chemical Name:methyl N-[3-(4-nitrophenyl)-2,2-trimethylenedithiopropionyl]-L-phenylalaninate
CAS No.:1297871-78-3
Molecular Formula:C₂₂H₂₄N₂O₅S₂
Molecular Weight:460.575
Hs Code.:

Synonyms:methyl N-[3-(4-nitrophenyl)-2,2-trimethylenedithiopropionyl]-L-phenylalaninate

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Chemical Property of methyl N-[3-(4-nitrophenyl)-2,2-trimethylenedithiopropionyl]-L-phenylalaninate

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Technology Process of methyl N-[3-(4-nitrophenyl)-2,2-trimethylenedithiopropionyl]-L-phenylalaninate

There total 4 articles about methyl N-[3-(4-nitrophenyl)-2,2-trimethylenedithiopropionyl]-L-phenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1297871-74-9
3-(4-nitrophenyl)-2,2-trimethylenedithiopropionic acid

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 1297871-78-3
methyl N-[3-(4-nitrophenyl)-2,2-trimethylenedithiopropionyl]-L-phenylalaninate

Guidance literature:: With 1,2-dichloro-ethane; triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.3998/ark.5550190.0012.316

Reference yield:

: 2-methyl-4(4-nitrophenylmethylene)-2-oxazolin-5-one

: 1297871-78-3
methyl N-[3-(4-nitrophenyl)-2,2-trimethylenedithiopropionyl]-L-phenylalaninate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / acetic acid / 6 °C / Reflux

2: boron trifluoride diethyl etherate / dichloromethane / 16 h / Reflux

3: 1,2-dichloro-ethane; triethylamine / dichloromethane / 24 h / 20 °C

With hydrogenchloride; boron trifluoride diethyl etherate; 1,2-dichloro-ethane; triethylamine; In dichloromethane; acetic acid;
DOI:10.3998/ark.5550190.0012.316

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1297871-78-3
methyl N-[3-(4-nitrophenyl)-2,2-trimethylenedithiopropionyl]-L-phenylalaninate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate; N-acetylglycine / 2 h / 80 - 85 °C

2: hydrogenchloride / acetic acid / 6 °C / Reflux

3: boron trifluoride diethyl etherate / dichloromethane / 16 h / Reflux

4: 1,2-dichloro-ethane; triethylamine / dichloromethane / 24 h / 20 °C

With hydrogenchloride; boron trifluoride diethyl etherate; sodium acetate; 1,2-dichloro-ethane; triethylamine; N-acetylglycine; In dichloromethane; acetic acid;
DOI:10.3998/ark.5550190.0012.316