1H-Imidazole-5-carboxaldehyde, 4-(1,1-dimethyl-2-propen-1-yl)-

Base Information

Chemical Name:1H-Imidazole-5-carboxaldehyde, 4-(1,1-dimethyl-2-propen-1-yl)-
CAS No.:316148-60-4
Molecular Formula:C9H12 N2 O
Molecular Weight:164.2
Hs Code.:
Mol file:316148-60-4.mol

Synonyms:1H-Imidazole-4-carboxaldehyde,5-(1,1-dimethyl-2-propenyl)- (9CI)

Suppliers and Price of 1H-Imidazole-5-carboxaldehyde, 4-(1,1-dimethyl-2-propen-1-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
4-(1,1-dimethyl-2-propen-1-yl)-1H-Imidazole-5-carboxaldehyde 97.00%
25G
$ 6000.00

AccelPharmtech
4-(1,1-dimethyl-2-propen-1-yl)-1H-Imidazole-5-carboxaldehyde 97.00%
1G
$ 1890.00

Total 1 raw suppliers

Chemical Property of 1H-Imidazole-5-carboxaldehyde, 4-(1,1-dimethyl-2-propen-1-yl)-

Chemical Property:

Melting Point:109-111 °C
Boiling Point:352.1±30.0 °C(Predicted)
PKA:11.20±0.10(Predicted)
PSA：45.75000
Density:1.087±0.06 g/cm3(Predicted)
LogP:1.68580

Purity/Quality:: 4-(1,1-dimethyl-2-propen-1-yl)-1H-Imidazole-5-carboxaldehyde 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Imidazole-5-carboxaldehyde, 4-(1,1-dimethyl-2-propen-1-yl)-

There total 13 articles about 1H-Imidazole-5-carboxaldehyde, 4-(1,1-dimethyl-2-propen-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 316148-59-1
(5-(1,1-dimethyl-2-propenyl)imidazole-4-yl)methanol

: 316148-60-4
5-(1,1-dimethyl-2-propenyl)imidazole-4-carbaldehyde

Guidance literature:: With manganese(IV) oxide; In acetone; at 20 ℃; for 1h;
DOI:10.1021/jo0012905

Reference yield: 85.0%

: 316148-59-1
[5-(1,1-dimethyl-allyl)-1H-imidazol-4-yl]-methanol

: 316148-60-4
5-(2-methylbut-3-en-2-yl)-1H-imidazole-4-carbaldehyde

Guidance literature:: With manganese(IV) oxide; In acetone; at 20 ℃; for 1.5h;
DOI:10.1016/j.tetlet.2009.09.074

Reference yield:

: 10276-09-2
2,2-dimethyl-but-3-enoic acid

: 316148-60-4
5-(1,1-dimethyl-2-propenyl)imidazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride; DMF / 20 - 80 °C

2: 8.1 g / n-BuLi / tetrahydrofuran; hexane / 1 h / -65 °C

3: 77 percent / sulfuryl chloride / CHCl₃ / Heating

4: 48 percent / H₂O / 4 h / 145 °C

5: 50 percent / DIBALH / toluene / 1 h / -30 °C

6: 95 percent / MnO₂ / acetone / 1 h / 20 °C

With manganese(IV) oxide; n-butyllithium; thionyl chloride; sulfuryl dichloride; diisobutylaluminium hydride; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; chloroform; water; acetone; toluene;
DOI:10.1021/jo0012905