(3,5-dibromophenyl)glycidol

Base Information

Chemical Name:(3,5-dibromophenyl)glycidol
CAS No.:937795-30-7
Molecular Formula:C₉H₈Br₂O₂
Molecular Weight:307.969
Hs Code.:

Synonyms:(3,5-dibromophenyl)glycidol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3,5-dibromophenyl)glycidol

Chemical Property:

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Technology Process of (3,5-dibromophenyl)glycidol

There total 3 articles about (3,5-dibromophenyl)glycidol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 352288-51-8
3-(3,5-dibromophenyl)prop-2-en-1-ol

: 937795-30-7
(3,5-dibromophenyl)glycidol

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; In 2,2,4-trimethylpentane; dichloromethane; at -20 ℃; for 3h;
DOI:10.1021/jo062612t

Reference yield:

: 352288-41-6
ethyl 3-(3,5-dibromophenyl)propenopate

: 937795-30-7
(3,5-dibromophenyl)glycidol

Guidance literature:: Multi-step reaction with 2 steps

1: DIBALH / diethyl ether; toluene / 1 h / 0 - 20 °C

2: L-DIPT; Ti(O-i-Pr)4; tert-butyl hydroperoxide / CH₂Cl₂; 2,2,4-trimethyl-pentane / 3 h / -20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; diisobutylaluminium hydride; In 2,2,4-trimethylpentane; diethyl ether; dichloromethane; toluene; 2: Sharpless epoxidation;
DOI:10.1021/jo062612t

Reference yield:

: 56990-02-4
3,5-dibromobenzaldehyde

: 937795-30-7
(3,5-dibromophenyl)glycidol

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / CH₂Cl₂ / Heating

2: DIBALH / diethyl ether; toluene / 1 h / 0 - 20 °C

3: L-DIPT; Ti(O-i-Pr)4; tert-butyl hydroperoxide / CH₂Cl₂; 2,2,4-trimethyl-pentane / 3 h / -20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; diisobutylaluminium hydride; In 2,2,4-trimethylpentane; diethyl ether; dichloromethane; toluene; 1: Wittig reaction / 3: Sharpless epoxidation;
DOI:10.1021/jo062612t