N,N'-bis<2'-(t-butoxycarbonyl)-(1'R,2'R)-diaminocyclohexyl>isophthalamide

Base Information

Chemical Name:N,N'-bis<2'-(t-butoxycarbonyl)-(1'R,2'R)-diaminocyclohexyl>isophthalamide
CAS No.:213765-35-6
Molecular Formula:C₃₀H₄₆N₄O₆
Molecular Weight:558.718
Hs Code.:

Synonyms:N,N'-bis<2'-(t-butoxycarbonyl)-(1'R,2'R)-diaminocyclohexyl>isophthalamide

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Chemical Property of N,N'-bis<2'-(t-butoxycarbonyl)-(1'R,2'R)-diaminocyclohexyl>isophthalamide

Chemical Property:

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Technology Process of N,N'-bis<2'-(t-butoxycarbonyl)-(1'R,2'R)-diaminocyclohexyl>isophthalamide

There total 3 articles about N,N'-bis<2'-(t-butoxycarbonyl)-(1'R,2'R)-diaminocyclohexyl>isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 146504-07-6
tert-butyl ((1R,2R)-2-aminocyclohexyl)carbamate

: 213765-35-6
N,N'-bis<2'-(t-butoxycarbonyl)-(1'R,2'R)-diaminocyclohexyl>isophthalamide

Guidance literature:: With triethylamine; In tetrahydrofuran; for 0.666667h; Ambient temperature;

Reference yield:

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 213765-35-6
N,N'-bis<2'-(t-butoxycarbonyl)-(1'R,2'R)-diaminocyclohexyl>isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / Et₃N / H₂O; dioxane / 4 h / Ambient temperature

2: 95 percent / Et₃N / tetrahydrofuran / 0.67 h / Ambient temperature

With triethylamine; In tetrahydrofuran; 1,4-dioxane; water;

Reference yield:

: 80994-44-1
{[(tert-butoxycarbonyl)oxy]amino}(phenyl)acetonitrile

: 213765-35-6
N,N'-bis<2'-(t-butoxycarbonyl)-(1'R,2'R)-diaminocyclohexyl>isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / Et₃N / H₂O; dioxane / 4 h / Ambient temperature

2: 95 percent / Et₃N / tetrahydrofuran / 0.67 h / Ambient temperature

With triethylamine; In tetrahydrofuran; 1,4-dioxane; water;