methyl syn-3-<(benzyloxycarbonyl)amino>-5-hydroxy-2-<(1-hydroxy-1-methyl)ethyl>pentanoate

Base Information

Chemical Name:methyl syn-3-<(benzyloxycarbonyl)amino>-5-hydroxy-2-<(1-hydroxy-1-methyl)ethyl>pentanoate
CAS No.:84787-53-1
Molecular Formula:C₁₇H₂₅NO₆
Molecular Weight:339.389
Hs Code.:

Synonyms:methyl syn-3-<(benzyloxycarbonyl)amino>-5-hydroxy-2-<(1-hydroxy-1-methyl)ethyl>pentanoate

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Chemical Property of methyl syn-3-<(benzyloxycarbonyl)amino>-5-hydroxy-2-<(1-hydroxy-1-methyl)ethyl>pentanoate

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Technology Process of methyl syn-3-<(benzyloxycarbonyl)amino>-5-hydroxy-2-<(1-hydroxy-1-methyl)ethyl>pentanoate

There total 4 articles about methyl syn-3-<(benzyloxycarbonyl)amino>-5-hydroxy-2-<(1-hydroxy-1-methyl)ethyl>pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77856-52-1
(S)-3-<(benzyloxycarbonyl)amino>-4-(methoxycarbonyl)butyric acid

: 84787-53-1
methyl syn-3-<(benzyloxycarbonyl)amino>-5-hydroxy-2-<(1-hydroxy-1-methyl)ethyl>pentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄

2: Ac₂O / pyridine

3: 77 percent / LDA / tetrahydrofuran / 1 h / -78 °C

4: 88 percent Turnov_. / hydrochloric acid

With hydrogenchloride; sodium tetrahydroborate; acetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; pyridine;
DOI:10.1021/ja00344a044

Reference yield:

: 84787-51-9,107173-68-2
((S)-2-Oxo-tetrahydro-pyran-4-yl)-carbamic acid benzyl ester

: 84787-53-1
methyl syn-3-<(benzyloxycarbonyl)amino>-5-hydroxy-2-<(1-hydroxy-1-methyl)ethyl>pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / LDA / tetrahydrofuran / 1 h / -78 °C

2: 88 percent Turnov_. / hydrochloric acid

With hydrogenchloride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ja00344a044

Reference yield:

: (S)-3-Benzyloxycarbonylamino-5-methoxy-pentanoic acid

: 84787-53-1
methyl syn-3-<(benzyloxycarbonyl)amino>-5-hydroxy-2-<(1-hydroxy-1-methyl)ethyl>pentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: Ac₂O / pyridine

2: 77 percent / LDA / tetrahydrofuran / 1 h / -78 °C

3: 88 percent Turnov_. / hydrochloric acid

With hydrogenchloride; acetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; pyridine;
DOI:10.1021/ja00344a044