4-amino-5-chloro-2-methoxy-N-((1-(6-phenylthiohexyl)piperidin-4-yl)methyl)benzamide

Base Information

• Chemical Name: 4-amino-5-chloro-2-methoxy-N-((1-(6-phenylthiohexyl)piperidin-4-yl)methyl)benzamide
• CAS No.: 188972-41-0
• Molecular Formula: C₂₆H₃₆ClN₃O₂S
• Molecular Weight: 490.11

Synonyms:4-amino-5-chloro-2-methoxy-N-((1-(6-phenylthiohexyl)piperidin-4-yl)methyl)benzamide

Chemical Property of 4-amino-5-chloro-2-methoxy-N-((1-(6-phenylthiohexyl)piperidin-4-yl)methyl)benzamide

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Technology Process of 4-amino-5-chloro-2-methoxy-N-((1-(6-phenylthiohexyl)piperidin-4-yl)methyl)benzamide

There total 3 articles about 4-amino-5-chloro-2-methoxy-N-((1-(6-phenylthiohexyl)piperidin-4-yl)methyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(6-chlorohexyl)(phenyl)sulfide (64740-56-3) + 4-(4-amino-5-chloro-2-methoxyphenylcarbonylamino-methyl)piperidine bis hydrochloride salt → 4-amino-5-chloro-2-methoxy-N-((1-(6-phenylthiohexyl)piperidin-4-yl)methyl)benzamide (188972-41-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; Heating;

DOI:10.1016/j.bmc.2005.02.016

Reference yield:

1-bromo-6-chlorohexane (6294-17-3) → 4-amino-5-chloro-2-methoxy-N-((1-(6-phenylthiohexyl)piperidin-4-yl)methyl)benzamide (188972-41-0)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide

2: K₂CO₃ / dimethylformamide / Heating

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2005.02.016

Reference yield:

thiophenol (108-98-5) → 4-amino-5-chloro-2-methoxy-N-((1-(6-phenylthiohexyl)piperidin-4-yl)methyl)benzamide (188972-41-0)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide

2: K₂CO₃ / dimethylformamide / Heating

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2005.02.016

upstream raw materials:

(6-chlorohexyl)(phenyl)sulfide

1-bromo-6-chlorohexane

thiophenol

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