C₂₅H₃₀N₂O₄S

Base Information

Chemical Name:C₂₅H₃₀N₂O₄S
CAS No.:1355952-12-3
Molecular Formula:C₂₅H₃₀N₂O₄S
Molecular Weight:454.59
Hs Code.:

C<sub>25</sub>H<sub>30</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:C₂₅H₃₀N₂O₄S

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Chemical Property of C₂₅H₃₀N₂O₄S

Chemical Property:

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Technology Process of C₂₅H₃₀N₂O₄S

There total 13 articles about C₂₅H₃₀N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1355951-90-4
C₃₁H₃₃N₃O₈S₂

: 1355952-12-3
C₂₅H₃₀N₂O₄S

Guidance literature:: With mercaptoacetic acid; lithium hydroxide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.5h;
DOI:10.1002/anie.201106205

Reference yield:

: 202753-56-8
2-(1H-4-bromoindol-3-yl)-ethanol

: 1355952-12-3
C₂₅H₃₀N₂O₄S

Guidance literature:: Multi-step reaction with 12 steps

1.1: dmap; triethylamine / dichloromethane / 10 h / 0 - 20 °C

2.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0.17 h / 20 °C

2.2: 0.67 h / 20 °C

3.1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4.1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C

5.1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

6.1: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

7.1: toluene-4-sulfonic acid / 3 h / 20 °C

8.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

9.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 20 °C

11.1: tributylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 0 - 20 °C

12.1: mercaptoacetic acid; lithium hydroxide / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

With dmap; lithium aluminium tetrahydride; thionyl chloride; sodium azide; tributylphosphine; methanesulfonamide; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; mercaptoacetic acid; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Heck reaction / 4.1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205

Reference yield:

: 1355951-84-6
C₂₈H₃₉NO₇S₂Si

: 1355952-12-3
C₂₅H₃₀N₂O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

2: toluene-4-sulfonic acid / 3 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

4: dmap; triethylamine / dichloromethane / 12 h / 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 20 °C

6: tributylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 0 - 20 °C

7: mercaptoacetic acid; lithium hydroxide / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

With dmap; lithium aluminium tetrahydride; sodium azide; tributylphosphine; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; toluene-4-sulfonic acid; mercaptoacetic acid; triethylamine; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201106205