2-(4-HYDROXY-3-METHOXY-PHENYL)-1H-BENZOIMIDAZOLE-4-CARBOXYLIC ACID

Base Information

Chemical Name:2-(4-HYDROXY-3-METHOXY-PHENYL)-1H-BENZOIMIDAZOLE-4-CARBOXYLIC ACID
CAS No.:313278-98-7
Molecular Formula:C15H12 N2 O4
Molecular Weight:284.27
Hs Code.:2933990090
Mol file:313278-98-7.mol

Synonyms:1H-Benzimidazole-4-carboxylicacid, 2-(4-hydroxy-3-methoxyphenyl)- (9CI)

Suppliers and Price of 2-(4-HYDROXY-3-METHOXY-PHENYL)-1H-BENZOIMIDAZOLE-4-CARBOXYLIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(4-HYDROXY-3-METHOXYPHENYL)-1H-1,3-BENZODIAZOLE-4-CARBOXYLIC ACID 95.00%
5MG
$ 498.08

Total 4 raw suppliers

Chemical Property of 2-(4-HYDROXY-3-METHOXY-PHENYL)-1H-BENZOIMIDAZOLE-4-CARBOXYLIC ACID

Chemical Property:

Vapor Pressure:9.87E-16mmHg at 25°C
Melting Point:299-302 °C
Refractive Index:1.714
Boiling Point:610°Cat760mmHg
PKA:1.90±0.10(Predicted)
Flash Point:322.7°C
PSA：95.44000
Density:1.455g/cm³
LogP:2.64230

Purity/Quality:

NLT 98% ^*data from raw suppliers

2-(4-HYDROXY-3-METHOXYPHENYL)-1H-1,3-BENZODIAZOLE-4-CARBOXYLIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(4-HYDROXY-3-METHOXY-PHENYL)-1H-BENZOIMIDAZOLE-4-CARBOXYLIC ACID

There total 2 articles about 2-(4-HYDROXY-3-METHOXY-PHENYL)-1H-BENZOIMIDAZOLE-4-CARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 121-33-5,8014-42-4
vanillin

: 603-81-6
2,3-diaminobenzoic acid

: 313278-98-7
2-(3'-methoxy-4'-hydroxyphenyl)-1H-benzimidazole-4-carboxylic acid

Guidance literature:: With copper diacetate; In methanol; water; Heating;
DOI:10.1021/jm000950v

Reference yield:

: 606-18-8
3-nitroanthranilic acid

: 313278-98-7
2-(3'-methoxy-4'-hydroxyphenyl)-1H-benzimidazole-4-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / H₂ / 10percent Pd/C / methanol / 760.05 Torr

2: 44 percent / Cu(OAc)2 / methanol; H₂O / Heating

With copper diacetate; hydrogen; 10percent Pd/C; In methanol; water;
DOI:10.1021/jm000950v