Technology Process of C30H32N2O7
There total 6 articles about C30H32N2O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
ethanol;
at 20 - 80 ℃;
for 30h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sodium carbonate / water; ethanol / 1 h / 0 °C / Inert atmosphere; Reflux
2: ethanol / 30 h / 20 - 80 °C / Inert atmosphere
With
hydroxylamine hydrochloride; sodium carbonate;
In
ethanol; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: boron tribromide / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
2: sodium iodide; potassium carbonate / N,N-dimethyl acetamide / 1 h / 50 °C / Inert atmosphere
3: sodium hydroxide; water / tetrahydrofuran; methanol / 1 h / 70 °C / Inert atmosphere
4: Jones reagent / acetone / 1 h / 0 °C / Inert atmosphere
5: ethanol / 30 h / 20 - 80 °C / Inert atmosphere
With
Jones reagent; water; boron tribromide; potassium carbonate; sodium iodide; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl acetamide; acetone;