{(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}B(C₆H₅)4

Base Information

• Chemical Name: {(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}B(C₆H₅)4
• CAS No.: 147243-76-3
• Molecular Formula: C₂₄H₂₀B*C₄₂H₄₃N₂OsP₄
• Molecular Weight: 1209.15

Synonyms:{(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}B(C₆H₅)4

Chemical Property of {(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}B(C₆H₅)4

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Technology Process of {(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}B(C₆H₅)4

There total 1 articles about {(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(N₂)}B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

{(P(CH2CH2P(C6H5)2)3)OsH2} (147243-71-8) + sodium tetraphenyl borate (143-66-8) + methyl trifluoromethanesulfonate (333-27-7) → {(P(CH2CH2P(C6H5)2)3)Os(H)(N2)}(1+)*B(C6H5)4(1-)={(P(CH2CH2P(C6H5)2)3)Os(H)(N2)}B(C6H5)4 (147243-76-3)

Guidance literature:

In tetrahydrofuran; N2;; EtOH added; crystd.; elem. anal.;;

Reference yield: 95.0%

{(P(CH2CH2P(C6H5)2)3)Os(H)(N2)}(1+)*B(C6H5)4(1-)={(P(CH2CH2P(C6H5)2)3)Os(H)(N2)}B(C6H5)4 (147243-76-3) → {(P(CH2CH2P(C6H5)2)3)Os(H)(CO)}(1+)*B(C6H5)4(1-)={(P(CH2CH2P(C6H5)2)3)Os(H)(CO)}B(C6H5)4 (147361-40-8)

Guidance literature:

With CO; In tetrahydrofuran; CO bubbled through soln. of complex for 5 min at room temp.;; concd.; crystd. from EtOH;;

Reference yield: 93.0%

{(P(C2H4P(C6H5)2)3)OsH(N2)}(1+)*B(C6H5)4(1-)={(P(C2H4P(C6H5)2)3)OsH(N2)}B(C6H5)4 (147243-76-3) + 1,4-bis(trimethylsilyl)-1,3-butadiyne (4526-07-2) → {P(C2H4P(C6H5)2)3Os((Si(CH3)3)C3CH(Si(CH3)3))}(1+)*B(C6H5)4(1-)={P(C2H4P(C6H5)2)3Os((Si(CH3)3)C3CH(Si(CH3)3))}B(C6H5)4

Guidance literature:

In tetrahydrofuran; addn. of Me3SiCCCCSiMe3 (0.51 mmol) to THF soln. of ((P(C2H4PPh2)3)OsH(N2))BPh4 (0.50 mmol); stirring for 1 h at room temp.; addn. of abs. ethanol;; crystn. on slow concn. under a stream of N2; elem. anal.;;

DOI:10.1016/0020-1693(94)03849-X

upstream raw materials:

{(P(CH₂CH₂P(C₆H₅)2)3)OsH₂}

sodium tetraphenyl borate

methyl trifluoromethanesulfonate

Downstream raw materials:

{(P(CH2CH2P(C6H5)2)3)Os(H)(η1-CO(CH3)2)}B(C6H5)4

{(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(CO)}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(CO)}B(C₆H₅)4

(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(OC(CH₃)2)⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(OC(CH₃)2)}B(C₆H₅)4

(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(OC(CH₃)CHCHC₆H₅)⁽¹⁺⁾*B(C₆H₅)4^(1-)={(P(CH₂CH₂P(C₆H₅)2)3)Os(H)(OC(CH₃)CHCHC₆H₅)}B(C₆H₅)4

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