36,37-diphenyl-2,5,11,14,19,22,28,31-octaoxa-8,25,35,38,43,45-hexaazaoctacyclo[30.15.2.1^35,38.0^15,41.0^18,40.0^33,47.0^36,45.0^37,43]pentaconta-1⁽⁴⁸⁾,15,17,32⁽⁴⁹⁾,33⁽⁴⁷⁾,40-hexaene-44,50-dione

Base Information

• Chemical Name: 36,37-diphenyl-2,5,11,14,19,22,28,31-octaoxa-8,25,35,38,43,45-hexaazaoctacyclo[30.15.2.1^35,38.0^15,41.0^18,40.0^33,47.0^36,45.0^37,43]pentaconta-1⁽⁴⁸⁾,15,17,32⁽⁴⁹⁾,33⁽⁴⁷⁾,40-hexaene-44,50-dione
• CAS No.: 124042-46-2
• Molecular Formula: C₄₈H₅₆N₆O₁₀
• Molecular Weight: 877.007

Synonyms:36,37-diphenyl-2,5,11,14,19,22,28,31-octaoxa-8,25,35,38,43,45-hexaazaoctacyclo[30.15.2.1^35,38.0^15,41.0^18,40.0^33,47.0^36,45.0^37,43]pentaconta-1⁽⁴⁸⁾,15,17,32⁽⁴⁹⁾,33⁽⁴⁷⁾,40-hexaene-44,50-dione

Chemical Property of 36,37-diphenyl-2,5,11,14,19,22,28,31-octaoxa-8,25,35,38,43,45-hexaazaoctacyclo[30.15.2.1^35,38.0^15,41.0^18,40.0^33,47.0^36,45.0^37,43]pentaconta-1⁽⁴⁸⁾,15,17,32⁽⁴⁹⁾,33⁽⁴⁷⁾,40-hexaene-44,50-dione

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Technology Process of 36,37-diphenyl-2,5,11,14,19,22,28,31-octaoxa-8,25,35,38,43,45-hexaazaoctacyclo[30.15.2.1^35,38.0^15,41.0^18,40.0^33,47.0^36,45.0^37,43]pentaconta-1⁽⁴⁸⁾,15,17,32⁽⁴⁹⁾,33⁽⁴⁷⁾,40-hexaene-44,50-dione

There total 1 articles about 36,37-diphenyl-2,5,11,14,19,22,28,31-octaoxa-8,25,35,38,43,45-hexaazaoctacyclo[30.15.2.1^35,38.0^15,41.0^18,40.0^33,47.0^36,45.0^37,43]pentaconta-1⁽⁴⁸⁾,15,17,32⁽⁴⁹⁾,33⁽⁴⁷⁾,40-hexaene-44,50-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1,3:4,6-bis<3,3':6,6'-bis(1,4,10,13-tetraoxa-7-benzyl-7-azatridecamethylene)-1,2-xylylene>tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione (124042-45-1) → 36,37-diphenyl-2,5,11,14,19,22,28,31-octaoxa-8,25,35,38,43,45-hexaazaoctacyclo[30.15.2.135,38.015,41.018,40.033,47.036,45.037,43]pentaconta-1(48),15,17,32(49),33(47),40-hexaene-44,50-dione (124042-46-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; at 55 ℃; for 168h; under 3040 Torr;

DOI:10.1021/jo00289a015

Reference yield: 76.0%

36,37-diphenyl-2,5,11,14,19,22,28,31-octaoxa-8,25,35,38,43,45-hexaazaoctacyclo[30.15.2.135,38.015,41.018,40.033,47.036,45.037,43]pentaconta-1(48),15,17,32(49),33(47),40-hexaene-44,50-dione (124042-46-2) + 21H,23H-5-(4-(3-bromopropyloxy)phenyl)-10,15,20-tris(4-methylphenyl)porphyrin → C148H136N14O12

Guidance literature:

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 100 ℃; for 120h;

DOI:10.1560/6CLA-J8W3-TDE1-CF5C

Reference yield: 60.0%

36,37-diphenyl-2,5,11,14,19,22,28,31-octaoxa-8,25,35,38,43,45-hexaazaoctacyclo[30.15.2.135,38.015,41.018,40.033,47.036,45.037,43]pentaconta-1(48),15,17,32(49),33(47),40-hexaene-44,50-dione (124042-46-2) + chloroacetyl chloride (79-04-9) → 2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis(α-chloroacetyl)-1H,4H-6,37:20,23-dietheno-2,22:3,21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopenta[cd]cyclotetra...

Guidance literature:

With TEA; In dichloromethane; at 20 ℃;

upstream raw materials:

1,3:4,6-bis<3,3':6,6'-bis(1,4,10,13-tetraoxa-7-benzyl-7-azatridecamethylene)-1,2-xylylene>tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

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