threo-N,N'-diisopropylamide of 2,3-diphenylsuccinic acid

Base Information

Chemical Name:threo-N,N'-diisopropylamide of 2,3-diphenylsuccinic acid
CAS No.:132401-10-6
Molecular Formula:C₂₂H₂₈N₂O₂
Molecular Weight:352.477
Hs Code.:

Synonyms:threo-N,N'-diisopropylamide of 2,3-diphenylsuccinic acid

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Chemical Property of threo-N,N'-diisopropylamide of 2,3-diphenylsuccinic acid

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Technology Process of threo-N,N'-diisopropylamide of 2,3-diphenylsuccinic acid

There total 3 articles about threo-N,N'-diisopropylamide of 2,3-diphenylsuccinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 132401-03-7
N,N'-diisopropyl-N,N'-di(phenylacetyl)hydrazine

: 132401-10-6
threo-N,N'-diisopropylamide of 2,3-diphenylsuccinic acid

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; 1.) -78 deg C, 20 min, 2.) 25 deg C, 60 min;
DOI:10.1039/c39900001686

Reference yield:

: 26254-05-7,76529-44-7,124891-86-7
N,N'-diisopropylohydrazine dihydrochloride

: 132401-10-6
threo-N,N'-diisopropylamide of 2,3-diphenylsuccinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Na₂CO₃ / H₂O / 1 h

2: 87 percent / lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 0.5 h / Heating

With sodium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; water;

Reference yield:

: 103-80-0
phenylacetyl chloride

: 132401-10-6
threo-N,N'-diisopropylamide of 2,3-diphenylsuccinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Na₂CO₃ / H₂O / 1 h

2: 87 percent / lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 0.5 h / Heating

With sodium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; water;