methyl 1-(cyclohex-1-enecarbonyl)-2-(4-methoxyphenyl)cyclopropanecarboxylate

Base Information

• Chemical Name: methyl 1-(cyclohex-1-enecarbonyl)-2-(4-methoxyphenyl)cyclopropanecarboxylate
• CAS No.: 1258517-96-2
• Molecular Formula: C₁₉H₂₂O₄
• Molecular Weight: 314.381

Synonyms:methyl 1-(cyclohex-1-enecarbonyl)-2-(4-methoxyphenyl)cyclopropanecarboxylate

Chemical Property of methyl 1-(cyclohex-1-enecarbonyl)-2-(4-methoxyphenyl)cyclopropanecarboxylate

Chemical Property:

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Technology Process of methyl 1-(cyclohex-1-enecarbonyl)-2-(4-methoxyphenyl)cyclopropanecarboxylate

There total 1 articles about methyl 1-(cyclohex-1-enecarbonyl)-2-(4-methoxyphenyl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

1-bromocyclohex-1-ene (2044-08-8) + methyl 1-(methoxy(methyl)carbamoyl)-2-(4-methoxyphenyl)cyclopropane-1-carboxylate (1258518-10-3) → methyl 1-(cyclohex-1-enecarbonyl)-2-(4-methoxyphenyl)cyclopropanecarboxylate (1258517-96-2)

Guidance literature:

1-bromocyclohex-1-ene; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; Inert atmosphere; Cooling with ice;

methyl 1-(methoxy(methyl)carbamoyl)-2-(4-methoxyphenyl)cyclopropane-1-carboxylate; In tetrahydrofuran; pentane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol102497w

Reference yield: 45.0%

methyl 1-(cyclohex-1-enecarbonyl)-2-(4-methoxyphenyl)cyclopropanecarboxylate (1258517-96-2) → methyl 4-(4-methoxyphenyl)-1-oxo-1,2,3,4,5,6,7,8-octahydronaphthalene-2-carboxylate (1258518-32-9) + methyl 1-hydroxy-4-(4-methoxyphenyl)-3,4,4a,5,6,7-hexahydronaphthalene-2-carboxylate

Guidance literature:

With indium(III) triflate; In dichloromethane; at 25 ℃; for 0.666667h; Inert atmosphere;

DOI:10.1021/ol102497w

upstream raw materials:

1-bromocyclohex-1-ene

methyl 1-(methoxy(methyl)carbamoyl)-2-(4-methoxyphenyl)cyclopropane-1-carboxylate

Downstream raw materials:

methyl 4-(4-methoxyphenyl)-1-oxo-1,2,3,4,5,6,7,8-octahydronaphthalene-2-carboxylate

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