1-Amino-3-methylpyridinium 2,4,6-trimethylbenzenesulfonate

Base Information

Chemical Name:1-Amino-3-methylpyridinium 2,4,6-trimethylbenzenesulfonate
CAS No.:55899-02-0
Molecular Formula:C₆H₉N₂*C₉H₁₁O₃S
Molecular Weight:308.401
Hs Code.:

Synonyms:SCHEMBL5384451;1-amino-3-methylpyridinium 2,4,6-trimethylbenzenesulfonate;DKJKTCMBLLHTEP-UHFFFAOYSA-M

Suppliers and Price of 1-Amino-3-methylpyridinium 2,4,6-trimethylbenzenesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Amino-3-methylpyridinium 2,4,6-trimethylbenzenesulfonate

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:308.11946368
Heavy Atom Count:21
Complexity:313

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C[N+](=CC=C1)N.CC1=CC(=C(C(=C1)C)S(=O)(=O)[O-])C

Technology Process of 1-Amino-3-methylpyridinium 2,4,6-trimethylbenzenesulfonate

There total 4 articles about 1-Amino-3-methylpyridinium 2,4,6-trimethylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-99-6
3-Methylpyridine

: 36016-40-7
mesitylenesulfonylhydroxylamine

: 55899-02-0
3-methyl-N-aminopyridinium mesitylenesulfonate

Guidance literature:: In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/ardp.200500227

Reference yield:

: 36016-39-4
N-(tert-butoxycarbonyl)-O-(mesitylsulfonyl)hydroxylamine

: 55899-02-0
3-methyl-N-aminopyridinium mesitylenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 0 °C / Inert atmosphere

2: dichloromethane / 0 °C / Inert atmosphere; Reflux

With trifluoroacetic acid; In dichloromethane;
DOI:10.1021/acs.orglett.2c00035

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 55899-02-0
3-methyl-N-aminopyridinium mesitylenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 70.1 percent / Et₃N / dimethylformamide / 0.5 h / 20 °C

2: aq. HClO₄ / dioxane / 0.33 h / -5 °C

3: CH₂Cl₂ / 1 h / 20 °C

With perchloric acid; triethylamine; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ardp.200500227