3-(4-methyl-2-oxo-2H-pyridin-1-yl)-5-tetrazol-1-yl-benzoic acid methyl ester

Base Information

Chemical Name:3-(4-methyl-2-oxo-2H-pyridin-1-yl)-5-tetrazol-1-yl-benzoic acid methyl ester
CAS No.:1000587-48-3
Molecular Formula:C₁₅H₁₃N₅O₃
Molecular Weight:311.3
Hs Code.:

Synonyms:3-(4-methyl-2-oxo-2H-pyridin-1-yl)-5-tetrazol-1-yl-benzoic acid methyl ester

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Chemical Property of 3-(4-methyl-2-oxo-2H-pyridin-1-yl)-5-tetrazol-1-yl-benzoic acid methyl ester

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Technology Process of 3-(4-methyl-2-oxo-2H-pyridin-1-yl)-5-tetrazol-1-yl-benzoic acid methyl ester

There total 5 articles about 3-(4-methyl-2-oxo-2H-pyridin-1-yl)-5-tetrazol-1-yl-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1000587-47-2
3-amino-5-(4-methyl-2-oxo-2H-pyridin-1-yl)benzoic acid methyl ester

: 122-51-0
orthoformic acid triethyl ester

: 1000587-48-3
3-(4-methyl-2-oxo-2H-pyridin-1-yl)-5-tetrazol-1-yl-benzoic acid methyl ester

Guidance literature:: With sodium azide; acetic acid; at 20 ℃; for 4h; Heating / reflux;

Reference yield:

: 121-92-6
3-nitrobenzoic acid

: 1000587-48-3
3-(4-methyl-2-oxo-2H-pyridin-1-yl)-5-tetrazol-1-yl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: iodine; sulfuric acid / 14 h / 85 °C

2: thionyl chloride / 2 h / 0 °C / Reflux

3: potassium phosphate; copper(l) iodide; 1,10-Phenanthroline / 1,4-dioxane / 24 h / 110 °C / Inert atmosphere

4: methanol; tin(ll) chloride / 3 h / Reflux

5: sodium azide; acetic acid / 4 h / Reflux

With methanol; potassium phosphate; copper(l) iodide; thionyl chloride; sodium azide; 1,10-Phenanthroline; sulfuric acid; iodine; acetic acid; tin(ll) chloride; In 1,4-dioxane;

Reference yield:

: 6313-17-3
3-iodo-5-nitro-benzoic acid

: 1000587-48-3
3-(4-methyl-2-oxo-2H-pyridin-1-yl)-5-tetrazol-1-yl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 2 h / 0 °C / Reflux

2: potassium phosphate; copper(l) iodide; 1,10-Phenanthroline / 1,4-dioxane / 24 h / 110 °C / Inert atmosphere

3: methanol; tin(ll) chloride / 3 h / Reflux

4: sodium azide; acetic acid / 4 h / Reflux

With methanol; potassium phosphate; copper(l) iodide; thionyl chloride; sodium azide; 1,10-Phenanthroline; acetic acid; tin(ll) chloride; In 1,4-dioxane;