Technology Process of C28H37NO10
There total 4 articles about C28H37NO10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
methyl (N-benzylbenzyloxycarbonyl-5-aminopentyl 4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-oct-2-ulopyranosid)onate;
With
sodium hydroxide;
In
1,4-dioxane; methanol; water;
at 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trimethylsilyl trifluoromethanesulfonate; silver trifluoroacetate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 1.5 h / Reflux; Inert atmosphere
3.1: sodium hydroxide / water; methanol; 1,4-dioxane / 20 °C / Inert atmosphere
3.2: Amberlite IR120 H+ resin
With
2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; tri-n-butyl-tin hydride; silver trifluoroacetate; sodium hydroxide;
In
1,4-dioxane; methanol; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 1.5 h / Reflux; Inert atmosphere
2.1: sodium hydroxide / water; methanol; 1,4-dioxane / 20 °C / Inert atmosphere
2.2: Amberlite IR120 H+ resin
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydroxide;
In
1,4-dioxane; methanol; water; toluene;
