chloromethyl (2S,3R)-<3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butyl> ether

Base Information

Chemical Name:chloromethyl (2S,3R)-<3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butyl> ether
CAS No.:148694-53-5
Molecular Formula:C₁₂H₁₆ClFOS
Molecular Weight:262.776
Hs Code.:

Synonyms:chloromethyl (2S,3R)-<3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butyl> ether

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Chemical Property of chloromethyl (2S,3R)-<3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butyl> ether

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Technology Process of chloromethyl (2S,3R)-<3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butyl> ether

There total 1 articles about chloromethyl (2S,3R)-<3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butyl> ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 114107-14-1
(2S,3R)-3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butanol

: 148694-53-5
chloromethyl (2S,3R)-<3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butyl> ether

Guidance literature:: With hydrogenchloride; In dichloromethane; at 0 ℃; for 4h;

Reference yield:

: 148694-53-5
chloromethyl (2S,3R)-<3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butyl> ether

: (2S,3R)-9-<(3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butoxy)methyl>adenine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) ammonium sulphate, hexamethyldisilazane, 2.) tetra-n-butylammonium iodide (TBAI) / 1.) reflux, 3 h, 2.) acetonitrile, reflux, 3 h

2: 95 percent / NH₃ (gas) / methanol / 12 h / 80 °C

With ammonium sulfate; ammonia; tetra-(n-butyl)ammonium iodide; 1,1,1,3,3,3-hexamethyl-disilazane; In methanol;

Reference yield:

: 148694-53-5
chloromethyl (2S,3R)-<3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butyl> ether

: 87-42-3
6-chloropurine

: 148694-63-7
(2S,3R)-6-chloro-9-<(3-fluoro-1-<(4-methylphenyl)sulphenyl>-2-butoxy)methyl>purine

Guidance literature:: With ammonium sulfate; tetra-(n-butyl)ammonium iodide; 1,1,1,3,3,3-hexamethyl-disilazane; Yield given. Multistep reaction; 1.) reflux, 3 h, 2.) acetonitrile, reflux, 3 h;