(S)-allyl-(5-(benzyloxy)-2-(2-(hydroxymethyl)pyrrolidine-1-carbonyl)-4-methoxyphenyl)carbamate

Base Information

Chemical Name:(S)-allyl-(5-(benzyloxy)-2-(2-(hydroxymethyl)pyrrolidine-1-carbonyl)-4-methoxyphenyl)carbamate
CAS No.:550356-49-5
Molecular Formula:C₂₄H₂₈N₂O₆
Molecular Weight:440.496
Hs Code.:

Synonyms:(S)-allyl-(5-(benzyloxy)-2-(2-(hydroxymethyl)pyrrolidine-1-carbonyl)-4-methoxyphenyl)carbamate

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Chemical Property of (S)-allyl-(5-(benzyloxy)-2-(2-(hydroxymethyl)pyrrolidine-1-carbonyl)-4-methoxyphenyl)carbamate

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Technology Process of (S)-allyl-(5-(benzyloxy)-2-(2-(hydroxymethyl)pyrrolidine-1-carbonyl)-4-methoxyphenyl)carbamate

There total 7 articles about (S)-allyl-(5-(benzyloxy)-2-(2-(hydroxymethyl)pyrrolidine-1-carbonyl)-4-methoxyphenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2937-50-0
Allyl chloroformate

: 260391-50-2
(2-amino-4-(benzyloxy)-5-methoxyphenyl)(2-(hydroxymethyl)pyrrolidin-1-yl)methanone

: 550356-49-5
(S)-allyl-(5-(benzyloxy)-2-(2-(hydroxymethyl)pyrrolidine-1-carbonyl)-4-methoxyphenyl)carbamate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1021/jm020526p

Reference yield:

: 60547-92-4
4-(benzyloxy)-5-methoxy-2-nitrobenzoic acid

: 550356-49-5
(S)-allyl-(5-(benzyloxy)-2-(2-(hydroxymethyl)pyrrolidine-1-carbonyl)-4-methoxyphenyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: (COCl)2 / dimethylformamide

2: K₂CO₃

3: SnCl₂

4: 81 percent / pyridine / CH₂Cl₂ / 0.17 h / 0 °C

With pyridine; oxalyl dichloride; potassium carbonate; tin(ll) chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020526p

Reference yield:

: 64154-78-5
4-benzyloxy-5-methoxy-2-nitrobenzoyl chloride

: 550356-49-5
(S)-allyl-(5-(benzyloxy)-2-(2-(hydroxymethyl)pyrrolidine-1-carbonyl)-4-methoxyphenyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃

2: SnCl₂

3: 81 percent / pyridine / CH₂Cl₂ / 0.17 h / 0 °C

With pyridine; potassium carbonate; tin(ll) chloride; In dichloromethane;
DOI:10.1021/jm020526p