2-METHYLPHENYLZINC IODIDE

Base Information

Chemical Name:2-METHYLPHENYLZINC IODIDE
CAS No.:312693-23-5
Molecular Formula:C₇H₇IZn
Molecular Weight:283.427
Hs Code.:
Mol file:312693-23-5.mol

Synonyms:2-METHYLPHENYLZINC IODIDE;2-METHYLPHENYLZINC IODIDE, 0.5M SOLUTION;2-methylphenylzinc iodide solution

Suppliers and Price of 2-METHYLPHENYLZINC IODIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
2-Methylphenylzinciodide
100mL
$ 426.00

Crysdot
2-Methylphenylzinciodide 95+%
100g
$ 588.00

American Custom Chemicals Corporation
2-METHYLPHENYLZINC IODIDE 95.00%
1L
$ 7969.50

American Custom Chemicals Corporation
2-METHYLPHENYLZINC IODIDE 95.00%
500ML
$ 5313.00

American Custom Chemicals Corporation
2-METHYLPHENYLZINC IODIDE 95.00%
100ML
$ 2760.45

Alfa Aesar
2-Methylphenylzinc iodide, 0.5M in THF, packaged under Argon in resealable ChemSeal? bottles
50ml
$ 180.00

Total 8 raw suppliers

Chemical Property of 2-METHYLPHENYLZINC IODIDE

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：0.00000
Density:g/cm³
LogP:2.67840
Sensitive.:Air & Light Sensitive

Purity/Quality:

99% ^*data from raw suppliers

2-Methylphenylzinciodide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:F,Xn
Statements: 14-19-22-36/38-40-36/37-11
Safety Statements: 16-26-33-36-36/37

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-METHYLPHENYLZINC IODIDE

There total 1 articles about 2-METHYLPHENYLZINC IODIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 615-37-2
ortho-methylphenyl iodide

: 7440-66-6
zinc

: 312693-23-5
2-methylphenylzinc iodide

Guidance literature:: zinc; With chloro-trimethyl-silane; ethylene dibromide; lithium chloride; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Inert atmosphere;

ortho-methylphenyl iodide; In tetrahydrofuran; Inert atmosphere; Reflux;
DOI:10.1021/jacs.8b05374

Reference yield: 81.0%

: 312693-23-5
2-methylphenylzinc iodide

: 85058-03-3
1-bromo-1-(methylsulfonyl)pentane

: (S)-1-methyl-2-(1-(methylsulfonyl)pentyl)benzene

Guidance literature:: 1-bromo-1-(methylsulfonyl)pentane; With (1,2-dimethoxyethane)dichloronickel(II); (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); In tetrahydrofuran; at -20 - 20 ℃; for 0.583333h; Sealed tube; Inert atmosphere;

2-methylphenylzinc iodide; In tetrahydrofuran; at -20 ℃; for 24h; enantioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1021/ja506885s

Reference yield: 80.0%

: 312693-23-5
2-methylphenylzinc iodide

: 85058-03-3
1-bromo-1-(methylsulfonyl)pentane

: (R)-1-methyl-2-(1-(methylsulfonyl)pentyl)benzene

Guidance literature:: 1-bromo-1-(methylsulfonyl)pentane; With (1,2-dimethoxyethane)dichloronickel(II); (S,S)-2,2'-isopropylidenebis(4-phenyl-2-oxazoline); In tetrahydrofuran; at -20 - 20 ℃; for 0.583333h; Sealed tube; Inert atmosphere;

2-methylphenylzinc iodide; In tetrahydrofuran; at -20 ℃; for 24h; enantioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1021/ja506885s