C₄₇H₇₃N₅O₉Si₂

Base Information

Chemical Name:C₄₇H₇₃N₅O₉Si₂
CAS No.:320748-85-4
Molecular Formula:C₄₇H₇₃N₅O₉Si₂
Molecular Weight:908.296
Hs Code.:

C<sub>47</sub>H<sub>73</sub>N<sub>5</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₄₇H₇₃N₅O₉Si₂

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Chemical Property of C₄₇H₇₃N₅O₉Si₂

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Technology Process of C₄₇H₇₃N₅O₉Si₂

There total 19 articles about C₄₇H₇₃N₅O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 320748-85-4
C₄₇H₇₃N₅O₉Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / imidazole / CH₂Cl₂ / 9 h

2: 86 percent / DMAP; K₂CO₃ / dimethylformamide / 21 h

3: 88 percent / Bu₃SnH; AcOH / Pd(PPh₃)4 / CH₂Cl₂ / 1 h / 0 °C

4: 319 mg / iPr₂NEt₃; FDPP / CH₂Cl₂ / 48 h

With 1H-imidazole; dmap; iPr₂NEt₃; pentafluorophenyl diphenyl-phosphinate; tri-n-butyl-tin hydride; potassium carbonate; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol006759x

Reference yield:

: 1119-34-2
L-arginine hydrochloride

: 320748-85-4
C₄₇H₇₃N₅O₉Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 79 percent / aq. NaOH / 0 °C

2.1: 63 percent / aq. NaOH / tetrahydrofuran / 12 h

3.1: isobutyl chloroformate; NMM / dimethylformamide / 0.02 h / -20 °C

3.2: 72 percent / NaBH₄ / H₂O; dimethylformamide / -20 - 20 °C

4.1: 81 percent / imidazole / CH₂Cl₂ / 9 h

5.1: 86 percent / DMAP; K₂CO₃ / dimethylformamide / 21 h

6.1: 88 percent / Bu₃SnH; AcOH / Pd(PPh₃)4 / CH₂Cl₂ / 1 h / 0 °C

7.1: 319 mg / iPr₂NEt₃; FDPP / CH₂Cl₂ / 48 h

With 4-methyl-morpholine; 1H-imidazole; dmap; sodium hydroxide; iPr₂NEt₃; pentafluorophenyl diphenyl-phosphinate; tri-n-butyl-tin hydride; potassium carbonate; acetic acid; isobutyl chloroformate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol006759x

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 320748-85-4
C₄₇H₇₃N₅O₉Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 63 percent / aq. NaOH / tetrahydrofuran / 12 h

2.1: isobutyl chloroformate; NMM / dimethylformamide / 0.02 h / -20 °C

2.2: 72 percent / NaBH₄ / H₂O; dimethylformamide / -20 - 20 °C

3.1: 81 percent / imidazole / CH₂Cl₂ / 9 h

4.1: 86 percent / DMAP; K₂CO₃ / dimethylformamide / 21 h

5.1: 88 percent / Bu₃SnH; AcOH / Pd(PPh₃)4 / CH₂Cl₂ / 1 h / 0 °C

6.1: 319 mg / iPr₂NEt₃; FDPP / CH₂Cl₂ / 48 h

With 4-methyl-morpholine; 1H-imidazole; dmap; sodium hydroxide; iPr₂NEt₃; pentafluorophenyl diphenyl-phosphinate; tri-n-butyl-tin hydride; potassium carbonate; acetic acid; isobutyl chloroformate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol006759x