3-Chlorobenzylzinc chloride

Base Information

Chemical Name:3-Chlorobenzylzinc chloride
CAS No.:312624-13-8
Molecular Formula:C₇H₆Cl₂Zn
Molecular Weight:226.421
Hs Code.:
DSSTox Substance ID:DTXSID70399099
Mol file:312624-13-8.mol

Synonyms:3-chlorobenzylzinc chloride;312624-13-8;1-chloro-3-methanidylbenzene;chlorozinc(1+);3-Chlorobenzylzinc chloride 0.5 M in Tetrahydrofuran;MFCD01319881;DTXSID70399099;AKOS016017984;3-Chlorobenzylzinc chloride, 0.5M in THF;J-018319

Suppliers and Price of 3-Chlorobenzylzinc chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
3-Chlorobenzylzinc chloride solution 0.5 M in THF
50ml
$ 209.00

Rieke Metals
3-Chlorobenzylzincchloride
100mL
$ 510.00

Rieke Metals
3-Chlorobenzylzincchloride
50mL
$ 316.00

American Custom Chemicals Corporation
3-CHLOROBENZYLZINC CHLORIDE 95.00%
1L
$ 8085.00

American Custom Chemicals Corporation
3-CHLOROBENZYLZINC CHLORIDE 95.00%
500ML
$ 5428.50

American Custom Chemicals Corporation
3-CHLOROBENZYLZINC CHLORIDE 95.00%
100ML
$ 2795.10

Total 12 raw suppliers

Chemical Property of 3-Chlorobenzylzinc chloride

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：0.00000
Density:g/cm³
LogP:3.34270
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:223.913797
Heavy Atom Count:10
Complexity:78

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-Chlorobenzylzinc chloride solution 0.5 M in THF ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:F,Xn
Statements: 19-22-36/38-40-36/37-11
Safety Statements: 16-26-33-36-36/37

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:[CH2-]C1=CC(=CC=C1)Cl.Cl[Zn+]

Technology Process of 3-Chlorobenzylzinc chloride

There total 1 articles about 3-Chlorobenzylzinc chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 620-20-2,130468-19-8
1-Chloro-3-chloromethyl-benzene

: 7440-66-6
zinc

: 312624-13-8
(3-chlorobenzyl)zinc(II) chloride

Guidance literature:: With chloro-trimethyl-silane; ethylene dibromide; lithium chloride; In tetrahydrofuran; at 70 ℃; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1055/s-0034-1379458

Reference yield: 81.0%

: 1207431-89-7
3-ethoxy-4-iodo-1H-pyrazole

: 312624-13-8
(3-chlorobenzyl)zinc(II) chloride

: 4-(3-chlorobenzyl)-3-ethoxy-1H-pyrazole

Guidance literature:: With palladium diacetate; XPhos; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere; Microwave irradiation;
DOI:10.1055/s-0034-1379458

Reference yield: 78.0%

: C₁₀H₈ClF₃N₂O₃S

: 312624-13-8
(3-chlorobenzyl)zinc(II) chloride

: 4-[(3-chlorophenyl)methyl]-1-(methoxymethyl)-7-(trifluoromethanesulfonyl)-1H-indazole

Guidance literature:: With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;